Synthesis, characterization, and thermal behavior of palladium(II) coordination compounds containing isonicotinamide
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Springer
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Resumo
Palladium(II) coordination compounds of general formula trans-[PdX(2)(isn)(2)], X = Cl(-) (1), N(3) (-) (2), SCN(-) (3), NCO(-) (4), isn = isonicotinamide; were synthesized and characterized in solid state by elemental analysis, infrared spectroscopy, and simultaneous TG-DTA. TG experiments reveal that the compounds 1-4 undergo thermal decomposition in three or four stages, yielding Pd(0) as final residue, according to calculus and identification by X-ray powder diffraction.
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Palladium(II), Isonicotinamide, TG-DTA, IR spectroscopy
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Inglês
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Journal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 106, n. 2, p. 375-378, 2011.
