On-line extraction and determination of carbofuran in raw milk by direct HPLC injection on an ISRP column
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Coorientador
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Editor
Vieweg
Tipo
Artigo
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Resumo
A method has been developed for extraction and determination of carbofuran in milk. The method involved direct injection of raw milk on to a human serum albumin dimethyloctyl-silica gel (HSA-Cs) column and the use of 80:20 (v/v) 0.01 M phosphate buffer pH 5.5 - acetonitrile as mobile phase. UV spectrophotometric detection was performed at 220 nm. Identification was based on retention time. Quantification was performed by automatic peak-area determination and was calibrated by use of an external standard.
Descrição
Palavras-chave
column liquid chromatography, carbofuran pesticides, on-line analysis of milk
Idioma
Inglês
Citação
Chromatographia. Wiesbaden: Vieweg, v. 47, n. 1-2, p. 81-83, 1998.
