Pre-concentration of Cd(II), Cr(III), Cu(II) and Ni(II) on a column packed with free carboxymethylcellulose (CMCH)
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Data
1997-12-01
Autores
Padilha, Pedro de Magalhães [UNESP]
Rocha, Julio Cesar [UNESP]
Campos, Joaquim T.S. [UNESP]
Moreira, José Celso [UNESP]
Federici, Cilene C. [UNESP]
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Resumo
Carboxymethylcellulose packed in to a glass column was used to pre-concentrate metallic cations from aqueous solutions. The pre-concentrated metal cations are directly eluted from the column using 5.0 mL of 1.0 mol L -1 hydrochloric acid. The optimum pre-concentration conditions are given (glass column, 16 cm length, 0.80 cm i.d., stationary phase height of 12 cm, flow-rate, 1.5 mL min -1). The recuperation efficiency achieved is greater than 95%, while the enrichment factor is 10 for 50 mL of solution (0.50 mg L -1 each).
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Palavras-chave
Adsorption, Carboxymethylcellulose, Pre-concentration
Como citar
Journal of the Brazilian Chemical Society, v. 8, n. 4, p. 333-337, 1997.