Desenvolvimento de um dispositivo para obtenção de monocristais de ligas à base de cobre
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This paper describes the drawing, construction and optimization of a device, which can be used to obtain single crystals of different metallic materials with melting point from 550 to 1050°C. Components of ease obtaining and of low cost were used. The device was based on the modified Bridgman technique and it was used to obtain single crystals of copper-based alloys. The temperature axial profiles and a difference less then 1% in the temperature between the wall and the center of the ceramic tube in the critical region for obtaining single crystals of good quality indicated that the oven presents a good thermal stability. Single crystals of CuZnAl and CuAlAg alloys of good quality were growth and characterized using optical microscopy and Laüe X-ray back reflection.
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Copper-based alloys, Modified Bridgman technique, Single crystal, alloy, aluminum derivative, copper complex, silver derivative, zinc derivative, cost benefit analysis, crystal structure, device, extraction, high temperature, melting point, quality control, technique, temperature dependence, thermostability, X ray crystallography
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Português
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Quimica Nova, v. 26, n. 5, p. 757-762, 2003.
