Synthesis of wurtzite ZnS nanoparticles using the microwave assisted solvothermal method

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dc.contributor.authorLa Porta, Felipe A. [UNESP]
dc.contributor.authorFerrer, Mateus M.
dc.contributor.authorDe Santana, Yuri V.B.
dc.contributor.authorRaubach, Cristiane W.
dc.contributor.authorLongo, Valéria M. [UNESP]
dc.contributor.authorSambrano, Júlio R. [UNESP]
dc.contributor.authorLongo, Elson [UNESP]
dc.contributor.authorAndrés, Juan
dc.contributor.authorLi, Máximo S.
dc.contributor.authorVarela, José Arana [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionUniv. Jaume i
dc.contributor.institutionUniversidade Federal de São Carlos (UFSCar)
dc.contributor.institutionUniversidade de São Paulo (USP)
dc.date.accessioned2014-05-27T11:28:55Z
dc.date.available2014-05-27T11:28:55Z
dc.date.issued2013-04-15
dc.description.abstractIn this article, we report the development of an efficient and rapid microwave assisted solvothermal (MAS) method to prepare wurtzite ZnS nanoparticles at 413 K using different precursors. The materials obtained were analyzed by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (MET) ultraviolet-visible (UV-vis) and photoluminescence (PL) measurements. The structure, surface chemical composition and optical properties were investigated as a function of the precursor. In addition, effects as well as merits of microwave heating on the processing and characteristics of ZnS nanoparticles obtained are reported. The possible formation mechanism and optical properties of these nanoparticles were also reported. © 2012 Elsevier B.V. All rights reserved.en
dc.description.affiliationInstituto de Química UNESP, PO Box 355, 14801-970 Araraquara, SP
dc.description.affiliationDepartment of Analytical and Physical Chemistry Univ. Jaume i, Castelló de la Plana 12071
dc.description.affiliationDepartamento de Química UFSCar, PO Box 676, 13565-905 São Carlos, SP
dc.description.affiliationLaboratório de Simulação Molecular UNESP, PO Box 473, 17033-360 Bauru, SP
dc.description.affiliationDepartamento de Física USP, PO Box 369, 13560-970 São Carlos, São Paulo
dc.description.affiliationUnespInstituto de Química UNESP, PO Box 355, 14801-970 Araraquara, SP
dc.description.affiliationUnespLaboratório de Simulação Molecular UNESP, PO Box 473, 17033-360 Bauru, SP
dc.format.extent153-159
dc.identifierhttp://dx.doi.org/10.1016/j.jallcom.2012.12.081
dc.identifier.citationJournal of Alloys and Compounds, v. 556, p. 153-159.
dc.identifier.doi10.1016/j.jallcom.2012.12.081
dc.identifier.issn0925-8388
dc.identifier.lattes6284168579617066
dc.identifier.scopus2-s2.0-84872381537
dc.identifier.urihttp://hdl.handle.net/11449/75111
dc.identifier.wosWOS:000315183600025
dc.language.isoeng
dc.relation.ispartofJournal of Alloys and Compounds
dc.relation.ispartofjcr3.779
dc.relation.ispartofsjr1,020
dc.rights.accessRightsAcesso restrito
dc.sourceScopus
dc.subjectMicrowave
dc.subjectNanoparticles
dc.subjectOptical properties
dc.subjectZnS
dc.subjectDifferent precursors
dc.subjectField emission scanning electron microscopy
dc.subjectFormation mechanism
dc.subjectMicrowave assisted
dc.subjectPhotoluminescence measurements
dc.subjectSolvothermal
dc.subjectSolvothermal method
dc.subjectSurface chemical composition
dc.subjectWurtzites
dc.subjectZnS nanoparticles
dc.subjectField emission microscopes
dc.subjectMicrowaves
dc.subjectPhotoelectrons
dc.subjectTransmission electron microscopy
dc.subjectX ray diffraction
dc.subjectX ray photoelectron spectroscopy
dc.subjectZinc sulfide
dc.titleSynthesis of wurtzite ZnS nanoparticles using the microwave assisted solvothermal methoden
dc.typeArtigo
dcterms.licensehttp://www.elsevier.com/about/open-access/open-access-policies/article-posting-policy
unesp.author.lattes6284168579617066[7]
unesp.campusUniversidade Estadual Paulista (Unesp), Instituto de Química, Araraquarapt

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