Show simple item record

dc.contributor.authorGonçalves Nunes, Wilhan Donizete [UNESP]
dc.contributor.authorMannochio Russo, Helena [UNESP]
dc.contributor.authorda Silva Bolzani, Vanderlan [UNESP]
dc.contributor.authorCaires, Flávio Junior [UNESP]
dc.date.accessioned2020-12-12T01:33:20Z
dc.date.available2020-12-12T01:33:20Z
dc.date.issued2020-01-01
dc.identifierhttp://dx.doi.org/10.1007/s10973-020-10104-3
dc.identifier.citationJournal of Thermal Analysis and Calorimetry.
dc.identifier.issn1588-2926
dc.identifier.issn1388-6150
dc.identifier.urihttp://hdl.handle.net/11449/199196
dc.description.abstractThe thermal behavior of two commercially available sweeteners based on Stevia rebaudiana Bertoni was studied by TG–DSC and EGA. The composition prior and after heating was analyzed by LC–MS/MS to identify the steviol glycosides present in each formulation and thermal degradation products, respectively. The two formulations (S1 and S2) presented thermal stability up to at least 200 °C. By DSC, it was possible to identify the presence of rebaudioside (REB) C and REB A in S1. S2 was composed mainly by erythritol (confirmed by both DSC and FTIR), REB A and E. By LC–MS/MS analyses, it was possible to observe that S1 is composed mainly by stevioside and REB A, E, C and B, and that the major products formed after heating are, basically, partially deglycosylated steviol structures. The thermal decomposition products were different depending on the formulation employed. These chemical changes in the compounds’ properties can cause a change in the desired taste and solubility of the formulations.en
dc.language.isoeng
dc.relation.ispartofJournal of Thermal Analysis and Calorimetry
dc.sourceScopus
dc.subjectDecomposition products
dc.subjectEGA
dc.subjectLC–MS/MS
dc.subjectStevia rebaudiana
dc.subjectTG–DSC
dc.titleThermal characterization and compounds identification of commercial Stevia rebaudiana Bertoni sweeteners and thermal degradation products at high temperatures by TG–DSC, IR and LC–MS/MSen
dc.typeArtigo
dc.contributor.institutionCiência e Tecnologia de Rondônia (IFRO)
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.description.affiliationInstituto Federal de Educação Ciência e Tecnologia de Rondônia (IFRO), Campus Ji-Paraná
dc.description.affiliationInstituto de Química Universidade Estadual Paulista (Unesp)
dc.description.affiliationFaculdade de Ciências Universidade Estadual Paulista (Unesp)
dc.description.affiliationUnespInstituto de Química Universidade Estadual Paulista (Unesp)
dc.description.affiliationUnespFaculdade de Ciências Universidade Estadual Paulista (Unesp)
dc.identifier.doi10.1007/s10973-020-10104-3
dc.identifier.scopus2-s2.0-85088875600
unesp.author.orcid0000-0002-0609-6678[1]
unesp.author.orcid0000-0002-4961-2353[2]
unesp.author.orcid0000-0001-7019-5825[3]
unesp.author.orcid0000-0003-3187-2111[4]
Localize o texto completo

Files in this item

FilesSizeFormatView

There are no files associated with this item.

This item appears in the following Collection(s)

Show simple item record