Pre-sintered Y-TZP sandblasting: effect on surface roughness, phase transformation, and Y-TZP/veneer bond strength

Carregando...
Imagem de Miniatura

Data

2017-11-01

Orientador

Coorientador

Pós-graduação

Curso de graduação

Título da Revista

ISSN da Revista

Título de Volume

Editor

Univ Sao Paulo Fac Odontologia Bauru

Tipo

Artigo

Direito de acesso

Acesso abertoAcesso Aberto

Resumo

Sandblasting is a common method to try to improve the Y-TZP/veneer bond strength of dental prostheses, however, it may put stress on zirconia surfaces and could accelerate the t -> m phase transformation. Y-TZP sandblasting before sintering could be an alternative to improve surface roughness and bonding strength of veneering ceramic. Objectives. The aim of this study was to analyze the effect of Y-TZP pre-sintering sandblasting on surface roughness, phase transformation, and the Y-TZP/veneer shear bond strength. Material and Methods. The Y-TZP specimen surface underwent sandblasting with aluminum oxide (50 mu m) pre-sintering (Z-PRE) and post sintering (Z-POS). Z-CTR was not subjected to surface treatment. After ceramic veneer application, the specimens were subjected to shear bond testing. Surface roughness was analyzed by confocal microscopy. Y-TZP monoclinic and tetragonal phases were evaluated by micro-Raman spectroscopy. Shear bond strength and surface roughness data were analyzed by One-way ANOVA and Tukey tests (alpha=0.05). Differences in the wave numbers and the broadening bands of the Raman spectra were compared among groups. Results. Z-POS (9.73 +/- 5.36 MPa) and Z-PRE (7.94 +/- 2.52 MPa) showed the highest bond strength, significantly higher than that of Z-CTR (5.54 +/- 2.14 MPa). The Ra of Z-PRE (1.59 +/- 0.23 mu m) was much greater and significantly different from that of Z-CTR (0.29 +/- 0.05 mu m) and Z-POS (0.77 +/- 0.13 mu m). All groups showed bands typical of the tetragonal (T) and monoclinic (M) phases. Y-TZP sandblasting before sintering resulted in rougher surfaces but did not increase the shear bond strength compared to post-sintering and increased surface defects. Conclusions. Surface treatment with Al3O2, regardless of the moment and application, improves the results of Y-TZP/veneer bonding and is not a specific cause of t -> m transformation.

Descrição

Idioma

Inglês

Como citar

Journal Of Applied Oral Science. Bauru-sp: Univ Sao Paulo Fac Odontologia Bauru, v. 25, n. 6, p. 666-673, 2017.

Itens relacionados