Synthesis, spectral and thermal studies on dicarboxylate-bridged palladium(II) coordination polymers. Part I

dc.contributor.authorFernandes, R. L. [UNESP]
dc.contributor.authorTakahashi, P. M. [UNESP]
dc.contributor.authorFrem, R. C. G. [UNESP]
dc.contributor.authorNetto, A. V. G. [UNESP]
dc.contributor.authorMauro, A. E.
dc.contributor.authorMatos, J. R.
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionUniversidade de São Paulo (USP)
dc.date.accessioned2014-05-20T14:20:12Z
dc.date.available2014-05-20T14:20:12Z
dc.date.issued2009-07-01
dc.description.abstractThis work describes the synthesis, IR and (13)C CPMAS NMR spectroscopic as well the thermal characterization of the new dicarboxylate complexes [Pd(2)(ox)(2)(4,4'-bipy)]n (1), [Pd(2)(ox)(2)(bpe)](n) (2) and [Pd(2)(ox)(2)(pz)](n) (3) {ox = oxalate, bipy = 4,4'-bipyridine, bpe = 1,2-bis(4-pyridyl)ethane, pz = pyrazine}. TG experiments reveal that compounds 1-3 undergo thermal decomposition in three steps. Metal palladium was the final product of the thermal decompositions, which was identified by X-ray powder diffraction.en
dc.description.affiliationUNESP, Inst Quim Araraquara, BR-14801970 Araraquara, SP, Brazil
dc.description.affiliationUSP SP, Inst Quim, São Paulo, Brazil
dc.description.affiliationUnespUNESP, Inst Quim Araraquara, BR-14801970 Araraquara, SP, Brazil
dc.format.extent123-126
dc.identifierhttp://dx.doi.org/10.1007/s10973-009-0252-8
dc.identifier.citationJournal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 97, n. 1, p. 123-126, 2009.
dc.identifier.doi10.1007/s10973-009-0252-8
dc.identifier.issn1388-6150
dc.identifier.lattes7927677053650819
dc.identifier.lattes8534138813417161
dc.identifier.orcid0000-0002-0057-7964
dc.identifier.orcid0000-0003-1574-681X
dc.identifier.urihttp://hdl.handle.net/11449/26067
dc.identifier.wosWOS:000270840800021
dc.language.isoeng
dc.publisherSpringer
dc.relation.ispartofJournal of Thermal Analysis and Calorimetry
dc.relation.ispartofjcr2.209
dc.relation.ispartofsjr0,587
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subject(13)C CPMAS NMRen
dc.subjectIRen
dc.subjectOxalateen
dc.subjectPalladium(II)en
dc.subjectThermal behavioren
dc.titleSynthesis, spectral and thermal studies on dicarboxylate-bridged palladium(II) coordination polymers. Part Ien
dc.typeArtigo
dcterms.licensehttp://www.springer.com/open+access/authors+rights?SGWID=0-176704-12-683201-0
dcterms.rightsHolderSpringer
unesp.author.lattes7927677053650819[4]
unesp.author.lattes3300223970814448[5]
unesp.author.lattes8534138813417161[3]
unesp.author.orcid0000-0002-0057-7964[4]
unesp.author.orcid0000-0002-1793-7735[6]
unesp.author.orcid0000-0003-1574-681X[3]

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