Corbi, P. P.Cavicchioli, M.Mel'nikov, P.Massabni, A. C.de Oliveira, LAA2014-05-202014-05-202000-01-01Russian Journal of Coordination Chemistry. New York: Maik Nauka/interperiodica, v. 26, n. 1, p. 28-31, 2000.1070-3284http://hdl.handle.net/11449/38385Cobalt(II) and nickel(II) djenkolates CoC7H12N2O4S2. H2O (I) and NiC7H12N2O4S2. H2O (II) were synthesized by the reaction of potassium djenkolate with the respective chlorides. LR spectra suggested coordination via the COO- and NH2 groups for the ligands in both compounds. Visible absorption spectra confirmed the octahedral structure of the complexes. X-ray powder diffraction patterns were indexed in the orthorhombic and monoclinic unit cells with parameters: a = 11.35, b = 7.35, c = 6.85 Angstrom for I and a = 11.54, b = 7.45, c = 6.90 Angstrom, beta = 94.95 degrees for II.28-31engArtigoWOS:000085656500006Acesso restrito