Calori-Domingues, Maria AntoniaRechdan, Rafael CondinoMoretti, AdemarGloria, Eduardo Micotti daZambello, Ivani ValariniCorrente, José Eduardo [UNESP]Dias, Carlos Tadeu dos Santos2014-05-202014-05-202010-01-01Química Nova. Sociedade Brasileira de Química, v. 33, n. 7, p. 1409-1495, 2010.0100-4042http://hdl.handle.net/11449/27622The variability in aflatoxin B1 concentration among peanut subsamples of 4 sample preparation procedures was evaluated. For each procedure, 18 samples were prepared involving dry comminuting/homogenization or dry roughly comminuting followed by the preparation of a aqueous slurry. Ten analytical samples were withdrawn from each sample/procedure and analyzed by thin layer chromatography. The coefficient of variation (CV%) among each set of 10 analytical samples was assumed to be associated with the sample preparation procedure. The procedure that made use of a subsample mill and preparation of a subsample slurry, showed lower variability (CV%) among the analytical subsamples.1409-1495porsample preparationaflatoxinvariabilityAvaliação de procedimentos de preparo de amostra de amendoim in natura para análise de aflatoxinasEvaluation of sample preparation procedures for aflatoxin analysis in raw peanutArtigo10.1590/S0100-40422010000700012S0100-40422010000700012Acesso abertoS0100-40422010000700012.pdf0000-0001-5478-4996