Efeito da termociclagem em diferentes soluções nas propriedades físicas e químicas dos materiais resinosos
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Data
2018-12-18
Autores
Alonso, Alexandre Abdalla [UNESP]
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Editor
Universidade Estadual Paulista (Unesp)
Resumo
Os estudos em laboratório devem ser realizados para verificar e comprovar a eficácia destes novos materiais, equipamentos, técnicas e tecnologias, e sendo considerados aprovados, uma outra etapa in vivo deverá ser realizada. O advento da odontologia adesiva já causou profundas mudanças na prática da odontologia. A proposta deste trabalho foi avaliar in vitro, o efeito da termociclagem, em diferentes temperaturas (5°C, 55°C), soluções (água destilada, óleo mineral), quantidade de ciclos (500, 5.000, 10.000), utilizando um material restaurador universal nanohíbrido fotopolimerizável contendo carga inorgânica em uma matriz de metacrilato e um sistema de cimentação à base de resina composta de polimerização dual. A finalidade da termociclagem é o envelhecimento dos materiais pelo mecanismo do “choque térmico”. O objetivo deste trabalho foi demonstrar se a termociclagem interfere ou não nas propriedades físicas e químicas destes materiais. Foram confeccionados 90 corpos de prova (cp) de cada material, cinco de cada grupo, (cpCRc = corpos de prova do cimento resinoso com Y-TZP, cpCRs= corpos de prova do cimento resinoso sem Y-TZP, e cpRC= corpos de prova da resina composta), que foram armazenados em água destilada, até o início da termociclagem. Estes espécimes receberam o tratamento térmico (nas distintas soluções) e após este evento foram realizadas as mensurações de massa, rugosidade, nanodureza e avaliações em MEV/ EDS, FTIR/UATR. Os dados obtidos foram submetidos ao teste Anova três fatores (α = 0,05). Os grupos cpCRc, cpCRs, cpRC não apresentaram alterações e ou modificações nas propriedades físicas e químicas dos materiais, independentemente do tipo de ciclagem, solução, temperatura e número de ciclos. Portanto, o uso da termociclagem, nas temperaturas de (5°C, 55°C), diferentes soluções (água destilada, óleo mineral), quantidade de ciclos (500, 5.000, 10.000) não foi observado o envelhecimento térmico para estes materiais.
Laboratory studies should be performed to verify and prove the efficacy of these new materials, equipment, techniques and technologies, and being considered approved, another in vivo step should be performed. The advent of adhesive dentistry has already caused profound changes in the practice of dentistry. The determination of bond strength of dentin adhesives is a matter of great importance and interest in our profession. The purpose of this work is to evaluate in vitro the effect of thermocycling at different temperatures (5 °C, 55 °C), solvents (distilled water, mineral oil), number of cycles (500, 5.000, 10.000) and a universal nano-hybrid restorative light-curing material with contains inorganic fillers in a methacrylate matrix and a dual-curing composite-based luting system for permanent adhesive luting. The purpose of thermocycling is thermal and hydrolytic degradation; and the objective of this work is to demonstrate if the thermocycling interferes or not in the study in the physical and chemical properties. A metal matrix was produced to make the specimens (sp). A total of 90 (sp) from each material, five from each group, were prepared (BFX-C = YTZP with resin cement sp, BFX-S = YTZP without resin cement sp, and GRD = composite resin specimens) which were stored in distilled water until the beginning of the thermocycling. The sp received the thermal treatment (the different solvents) and after this event were reached the messages of mass, roughness, hardness. and evaluations in SEM / EDS, FTIR / UATR. Data were obtained from the Anova test (α = 0.05). The groups BFX-C, BFX-S, GRD are the parameters keys and physical properties of the materials, regardless of the type of cycling, solvent, temperature and number of cycles. Therefore, the use of thermocycling, at temperatures of 5 °C, 55 °C, different solvents, mineral oil, amount of heat (500, 5,000, 10,000) was not observed in the thermal heat for these materials.
Laboratory studies should be performed to verify and prove the efficacy of these new materials, equipment, techniques and technologies, and being considered approved, another in vivo step should be performed. The advent of adhesive dentistry has already caused profound changes in the practice of dentistry. The determination of bond strength of dentin adhesives is a matter of great importance and interest in our profession. The purpose of this work is to evaluate in vitro the effect of thermocycling at different temperatures (5 °C, 55 °C), solvents (distilled water, mineral oil), number of cycles (500, 5.000, 10.000) and a universal nano-hybrid restorative light-curing material with contains inorganic fillers in a methacrylate matrix and a dual-curing composite-based luting system for permanent adhesive luting. The purpose of thermocycling is thermal and hydrolytic degradation; and the objective of this work is to demonstrate if the thermocycling interferes or not in the study in the physical and chemical properties. A metal matrix was produced to make the specimens (sp). A total of 90 (sp) from each material, five from each group, were prepared (BFX-C = YTZP with resin cement sp, BFX-S = YTZP without resin cement sp, and GRD = composite resin specimens) which were stored in distilled water until the beginning of the thermocycling. The sp received the thermal treatment (the different solvents) and after this event were reached the messages of mass, roughness, hardness. and evaluations in SEM / EDS, FTIR / UATR. Data were obtained from the Anova test (α = 0.05). The groups BFX-C, BFX-S, GRD are the parameters keys and physical properties of the materials, regardless of the type of cycling, solvent, temperature and number of cycles. Therefore, the use of thermocycling, at temperatures of 5 °C, 55 °C, different solvents, mineral oil, amount of heat (500, 5,000, 10,000) was not observed in the thermal heat for these materials.
Descrição
Palavras-chave
Cimentos adesivos, Resinas compostas, Degradação hidrolítica, Espectroscopia no infravermelho - Fourier, Termociclagem, Adhesive cements, Composite resins, Hydrolytic degradation, Infrared spectroscopy – Fourier, Thermocycling