Characterization of chemically treated Ti-Zr system alloys for dental implant application

dc.contributor.authorCordeiro, Jairo M.
dc.contributor.authorFaverani, Leonardo P. [UNESP]
dc.contributor.authorGrandini, Carlos R. [UNESP]
dc.contributor.authorRangel, Elidiane C. [UNESP]
dc.contributor.authorda Cruz, Nilson C. [UNESP]
dc.contributor.authorNociti Junior, Francisco H.
dc.contributor.authorAlmeida, Amanda B.
dc.contributor.authorVicente, Fabio B.
dc.contributor.authorMorais, Bruna R.G. [UNESP]
dc.contributor.authorBarão, Valentim A.R.
dc.contributor.authorAssunção, Wirley G. [UNESP]
dc.contributor.institutionUniversidade Estadual de Campinas (UNICAMP)
dc.contributor.institutionTribocorrosion and Nanomedicine (IBTN)
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionUniversidade Paulista (UNIP)
dc.date.accessioned2018-12-11T17:21:41Z
dc.date.available2018-12-11T17:21:41Z
dc.date.issued2018-11-01
dc.description.abstractMaterials and surfaces developed for dental implants need to withstand degradation processes that take place in the oral cavity. Therefore, the aim of the study was to develop and evaluate the topographical, mechanical, chemical, electrochemical and biological properties of Ti-xZr alloys (x = 5, 10, and 15 wt%) with two surface features (machined and double acid etched). Commercially pure titanium (cpTi) and Ti-6Al-4V alloy were used as controls. Surface characterization was performed using dispersive energy spectroscopy, X-ray diffraction, scanning electron microscopy, atomic force microscopy, profilometry and surface energy. The mechanical properties were assessed using Vickers microhardness, elastic modulus and stiffness. The electrochemical behavior analysis was conducted in a body fluid solution (pH 7.4). In addition, MC3T3-E1 cells were used to determine the impact of material and surface treatment on cell morphology by SEM analysis. Data were analyzed by two-way ANOVA and Bonferroni test (α = 0.05). Ti-Zr alloys showed lower surface roughness, elastic modulus and stiffness, as well as higher hardness and surface energy when compared to cpTi. Ti-Zr system increased the polarization resistance values and significantly decreased the capacitance, corrosion current density (icorr), and passivation current density (ipass) values. The acid treatment increased the resistance and corrosion potential of the oxide layer. SEM data analysis demonstrated that Ti-Zr alloys displayed normal cell attachment/spreading and slightly changed cell morphology in the double etched surface. In conclusion, Zr addition and surface treatment altered surface, mechanical, biological and electrochemical properties of Ti material.en
dc.description.affiliationUniversity of Campinas (UNICAMP) Piracicaba Dental School Department of Prosthodontics and Periodontology, Av Limeira, 901
dc.description.affiliationInstitute of Biomaterials Tribocorrosion and Nanomedicine (IBTN)
dc.description.affiliationUniv Estadual Paulista (UNESP) Aracatuba Dental School Department of Surgery and Integrated Clinic, R. José Bonifácio, 1193
dc.description.affiliationUniv Estadual Paulista (UNESP) Laboratório de Anelasticidade e Biomateriais, Av. Eng. Luiz Edmundo Carrijo Coube
dc.description.affiliationUniv Estadual Paulista (UNESP) ICTS Laboratory of Technological Plasmas, Av Três de Março, 511
dc.description.affiliationUniversidade Paulista (UNIP), Av. Luís Levorato, 1-40
dc.description.affiliationUniv Estadual Paulista (UNESP) Aracatuba Dental School Department of Dental Materials and Prosthodontics, R. José Bonifácio, 1193
dc.description.affiliationUnespUniv Estadual Paulista (UNESP) Aracatuba Dental School Department of Surgery and Integrated Clinic, R. José Bonifácio, 1193
dc.description.affiliationUnespUniv Estadual Paulista (UNESP) Laboratório de Anelasticidade e Biomateriais, Av. Eng. Luiz Edmundo Carrijo Coube
dc.description.affiliationUnespUniv Estadual Paulista (UNESP) ICTS Laboratory of Technological Plasmas, Av Três de Março, 511
dc.description.affiliationUnespUniv Estadual Paulista (UNESP) Aracatuba Dental School Department of Dental Materials and Prosthodontics, R. José Bonifácio, 1193
dc.description.sponsorshipFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
dc.description.sponsorshipConselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
dc.description.sponsorshipIdFAPESP: 2013/08451-1
dc.description.sponsorshipIdFAPESP: 2013/15545-2
dc.description.sponsorshipIdFAPESP: 2014/23575-1
dc.description.sponsorshipIdFAPESP: 2015/03159-6
dc.description.sponsorshipIdFAPESP: 2015/25562-7
dc.description.sponsorshipIdFAPESP: 2016/11470-6
dc.description.sponsorshipIdCNPq: 311203/2013-2
dc.format.extent849-861
dc.identifierhttp://dx.doi.org/10.1016/j.msec.2018.07.046
dc.identifier.citationMaterials Science and Engineering C, v. 92, p. 849-861.
dc.identifier.doi10.1016/j.msec.2018.07.046
dc.identifier.file2-s2.0-85050154016.pdf
dc.identifier.issn0928-4931
dc.identifier.scopus2-s2.0-85050154016
dc.identifier.urihttp://hdl.handle.net/11449/176606
dc.language.isoeng
dc.relation.ispartofMaterials Science and Engineering C
dc.relation.ispartofsjr1,110
dc.rights.accessRightsAcesso aberto
dc.sourceScopus
dc.subjectAlloys
dc.subjectCorrosion
dc.subjectDental implant
dc.subjectTitanium
dc.subjectZirconium
dc.titleCharacterization of chemically treated Ti-Zr system alloys for dental implant applicationen
dc.typeArtigo
unesp.author.lattes2949983867418338[3]
unesp.author.orcid0000-0002-3336-309X[3]

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