Synthesis, characterization and thermal behaviour of light trivalent lanthanides folates on solid state

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dc.contributor.authorDametto, P. R. [UNESP]
dc.contributor.authorCaires, Flavio J. [UNESP]
dc.contributor.authorAmbrozini, B. [UNESP]
dc.contributor.authorIonashiro, Massao [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2014-05-20T15:32:14Z
dc.date.available2014-05-20T15:32:14Z
dc.date.issued2011-09-01
dc.description.abstractSolid state Ln(2)-L(3) compounds, where Ln stands for light trivalent lanthanides (lanthanum to gadolinium), except promethium, and L is folate (C(19)H(17)N(7)O(6)), have been synthesized. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy (FTIR), TG coupled to FTIR, elemental analysis and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results provided information concerning the stoichiometry, crystallinity, ligand's denticity, thermal stability, thermal behaviour and identification of the gaseous products evolved during the thermal decomposition of these compounds.en
dc.description.affiliationUNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil
dc.description.affiliationUnespUNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil
dc.description.sponsorshipFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
dc.description.sponsorshipConselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
dc.description.sponsorshipCoordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
dc.format.extent831-836
dc.identifierhttp://dx.doi.org/10.1007/s10973-010-1233-7
dc.identifier.citationJournal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 105, n. 3, p. 831-836, 2011.
dc.identifier.doi10.1007/s10973-010-1233-7
dc.identifier.issn1388-6150
dc.identifier.lattes8460531302083773
dc.identifier.urihttp://hdl.handle.net/11449/41195
dc.identifier.wosWOS:000294014000011
dc.language.isoeng
dc.publisherSpringer
dc.relation.ispartofJournal of Thermal Analysis and Calorimetry
dc.relation.ispartofjcr2.209
dc.relation.ispartofsjr0,587
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectLight lanthanidesen
dc.subjectFolateen
dc.subjectCharacterizationen
dc.subjectThermal behaviouren
dc.titleSynthesis, characterization and thermal behaviour of light trivalent lanthanides folates on solid stateen
dc.typeArtigo
dcterms.licensehttp://www.springer.com/open+access/authors+rights?SGWID=0-176704-12-683201-0
dcterms.rightsHolderSpringer
unesp.author.lattes8460531302083773
unesp.campusUniversidade Estadual Paulista (Unesp), Instituto de Química, Araraquarapt

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Artigos - Química Analítica - IQ