On-line extraction and determination of carbofuran in raw milk by direct HPLC injection on an ISRP column

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dc.contributor.authorMenezes, Manoel Lima de [UNESP]
dc.contributor.authorFelix, G.
dc.contributor.authorDemarchi, ACCO
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionENSCPB
dc.contributor.institutionUSC
dc.date.accessioned2014-05-20T15:20:43Z
dc.date.available2014-05-20T15:20:43Z
dc.date.issued1998-01-01
dc.description.abstractA method has been developed for extraction and determination of carbofuran in milk. The method involved direct injection of raw milk on to a human serum albumin dimethyloctyl-silica gel (HSA-Cs) column and the use of 80:20 (v/v) 0.01 M phosphate buffer pH 5.5 - acetonitrile as mobile phase. UV spectrophotometric detection was performed at 220 nm. Identification was based on retention time. Quantification was performed by automatic peak-area determination and was calibrated by use of an external standard.en
dc.description.affiliationUNESP, Fac Ciências, Dept Quim, BR-17033360 São Paulo, Brazil
dc.description.affiliationENSCPB, CNRS URA, Chim Organ & Organomet Lab, F-33402 Talence, France
dc.description.affiliationUSC, Lab Bioquim, BR-17044160 São Paulo, Brazil
dc.description.affiliationUnespUNESP, Fac Ciências, Dept Quim, BR-17033360 São Paulo, Brazil
dc.format.extent81-83
dc.identifierhttp://dx.doi.org/10.1007/BF02466790
dc.identifier.citationChromatographia. Wiesbaden: Vieweg, v. 47, n. 1-2, p. 81-83, 1998.
dc.identifier.doi10.1007/BF02466790
dc.identifier.issn0009-5893
dc.identifier.lattes4659698040759224
dc.identifier.urihttp://hdl.handle.net/11449/31962
dc.identifier.wosWOS:000071631000013
dc.language.isoeng
dc.publisherVieweg
dc.relation.ispartofChromatographia
dc.relation.ispartofjcr1.401
dc.relation.ispartofsjr0,514
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectcolumn liquid chromatographypt
dc.subjectcarbofuran pesticidespt
dc.subjecton-line analysis of milkpt
dc.titleOn-line extraction and determination of carbofuran in raw milk by direct HPLC injection on an ISRP columnen
dc.typeArtigo
dcterms.licensehttp://www.springer.com/open+access/authors+rights
dcterms.rightsHolderVieweg
unesp.author.lattes4659698040759224
unesp.campusUniversidade Estadual Paulista (Unesp), Faculdade de Ciências, Baurupt
unesp.departmentQuímica - FCpt

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