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Qualitative determination of indole alkaloids, triterpenoids and steroid of Tabernaemontana hilariana

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dc.contributor.authorCardoso, CAL
dc.contributor.authorVilegas, Wagner [UNESP]
dc.contributor.authorHonda, N. K.
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionUniversidade Federal de Mato Grosso do Sul (UFMS)
dc.date.accessioned2014-05-20T15:21:26Z
dc.date.available2014-05-20T15:21:26Z
dc.date.issued1998-05-29
dc.description.abstractThis paper reports the separation and identification of indole alkaloids, steroids and triterpenoids from the ethanolic extracts of Tabernaemontana hilariana (Apocynaceae). The alkaloidal fractions from the ethanolic extracts obtained (root barks, green fruits, ripe fruits and seeds) were fractionated and analysed by thin-layer chromatography, capillary gas chromatography-flame ionization detection (cGC-FID) as well as by high-resolution gas chromatography-mass spectrometry (HRGC-MS). 3-Hydroxycoronaridine, ibogamine, coronaridine pseudoindoxyl, coronaridine, catharanthine, voacangine hydroxyindolenine, voacangine pseudoindoxyl, tabernanthine, tetraphyllicine, 3-hydroxyvoacangine, voacangine, isovoacangine and 3-oxocoronaridine were identified. The insoluble fraction of ethanolic extracts obtained from the root barks and green fruits were analysed and ten aliphatic constituents were also identified by cGC-FID and HRGC-MS. (C) 1998 Elsevier B.V. B.V. All rights reserved.en
dc.description.affiliationUniv Estadual Paulista, Inst Quim Araraquara, Dept Quim Organ, BR-14800900 Araraquara, SP, Brazil
dc.description.affiliationUniv Estadual Paulista, Inst Quim Araraquara, Dept Quim Analit, BR-14800900 Araraquara, SP, Brazil
dc.description.affiliationUniv Fed Mato Grosso Sul, Dept Quim, BR-79070900 Campo Grande, MS, Brazil
dc.description.affiliationUnespUniv Estadual Paulista, Inst Quim Araraquara, Dept Quim Organ, BR-14800900 Araraquara, SP, Brazil
dc.description.affiliationUnespUniv Estadual Paulista, Inst Quim Araraquara, Dept Quim Analit, BR-14800900 Araraquara, SP, Brazil
dc.format.extent264-268
dc.identifierhttp://dx.doi.org/10.1016/S0021-9673(98)00084-3
dc.identifier.citationJournal of Chromatography A. Amsterdam: Elsevier B.V., v. 808, n. 1-2, p. 264-268, 1998.
dc.identifier.doi10.1016/S0021-9673(98)00084-3
dc.identifier.issn0021-9673
dc.identifier.orcid0000-0003-3032-2556
dc.identifier.urihttp://hdl.handle.net/11449/32585
dc.identifier.wosWOS:000074138500029
dc.language.isoeng
dc.publisherElsevier B.V.
dc.relation.ispartofJournal of Chromatography A
dc.relation.ispartofjcr3.716
dc.relation.ispartofsjr1,378
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectTabernaemontana hilarianapt
dc.subjectplant materialspt
dc.subjectindolespt
dc.subjectalkaloidspt
dc.subjecttriterpenoidspt
dc.subjectsteroidspt
dc.titleQualitative determination of indole alkaloids, triterpenoids and steroid of Tabernaemontana hilarianaen
dc.typeArtigo
dcterms.licensehttp://www.elsevier.com/about/open-access/open-access-policies/article-posting-policy
dcterms.rightsHolderElsevier B.V.
dspace.entity.typePublication
unesp.author.orcid0000-0003-3032-2556[2]
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
unesp.departmentQuímica Analítica - IQARpt
unesp.departmentQuímica Orgânica - IQARpt

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Araraquara - IQAR - Instituto de Química