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Development, optimization and validation of gas chromatographic fingerprinting of Brazilian commercial gasoline for quality control

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dc.contributor.authorFlumignan, Danilo Luiz [UNESP]
dc.contributor.authorFerreira, Fabricio de Oliveira [UNESP]
dc.contributor.authorTininis, Aristeu Gomes [UNESP]
dc.contributor.authorLopes, Márcia Nasser [UNESP]
dc.contributor.authorOliveira, Jose Eduardo de [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2014-05-20T14:21:13Z
dc.date.available2014-05-20T14:21:13Z
dc.date.issued2008-08-22
dc.description.abstractThree-step development, optimization and validation strategy for GC fingerprints of Brazilian commercial gasoline is described. A suitable chromatographic system was selected first. The following step was to improve acceptable chromatographic resolution with reduced analysis time, which is recommended for routine applications. Optimization was carried out using full three-level factorial designs. Optimal conditions were obtained for flow rate, oven ramps, injection volume and split ratio. Finally, several validation parameters were performed. Therefore, a feasible and reliable fingerprint was established to identify Brazilian commercial gasoline quality. This strategy can also be applied to develop fingerprints for quality control of other fuels. (C) 2008 Elsevier B.V. All rights reserved.en
dc.description.affiliationSão Paulo State Univ UNESP, Inst Chem, Dept Organ Chem, Ctr Monitoring & Res Qual Fuels Biofuels Crude Oi, BR-14800900 Araraquara, SP, Brazil
dc.description.affiliationUnespSão Paulo State Univ UNESP, Inst Chem, Dept Organ Chem, Ctr Monitoring & Res Qual Fuels Biofuels Crude Oi, BR-14800900 Araraquara, SP, Brazil
dc.description.sponsorshipAgência Nacional do Petróleo, Gás Natural e Biocombustíveis (ANP)
dc.description.sponsorshipGAS Natural e Biocombustiveis-ANP
dc.description.sponsorshipFundação para o Desenvolvimento da UNESP (FUNDUNESP)
dc.description.sponsorshipCoordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
dc.description.sponsorshipConselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
dc.description.sponsorshipCEMPEQC (Centro de Monitoramento e Pesquisa na Qualidade de Combustiveis, Biocombustiveis, Petroleo e Derivaclos)
dc.format.extent181-188
dc.identifierhttp://dx.doi.org/10.1016/j.chroma.2008.06.040
dc.identifier.citationJournal of Chromatography A. Amsterdam: Elsevier B.V., v. 1202, n. 2, p. 181-188, 2008.
dc.identifier.doi10.1016/j.chroma.2008.06.040
dc.identifier.issn0021-9673
dc.identifier.lattes3310170899693944
dc.identifier.lattes9352141379363877
dc.identifier.urihttp://hdl.handle.net/11449/26348
dc.identifier.wosWOS:000258696800010
dc.language.isoeng
dc.publisherElsevier B.V.
dc.relation.ispartofJournal of Chromatography A
dc.relation.ispartofjcr3.716
dc.relation.ispartofsjr1,378
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectgas chromatographic fingerprintingen
dc.subjectmethod developmenten
dc.subjectresponse surface methodologyen
dc.subjectBrazilian commercial gasolineen
dc.subjectquality controlen
dc.titleDevelopment, optimization and validation of gas chromatographic fingerprinting of Brazilian commercial gasoline for quality controlen
dc.typeArtigo
dcterms.licensehttp://www.elsevier.com/about/open-access/open-access-policies/article-posting-policy
dcterms.rightsHolderElsevier B.V.
dspace.entity.typePublication
unesp.author.lattes3310170899693944
unesp.author.lattes9352141379363877
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
unesp.departmentQuímica Orgânica - IQARpt

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