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Synthesis, characterization and thermal decomposition of [Pd2 (C2-dmba) (μ-SO4) (μ-SO4) SO22]

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dc.contributor.authorCaires, Antonio Carlos Fávero
dc.contributor.authorMauro, Antonio Eduardo [UNESP]
dc.contributor.institutionUniversidade Federal do Rio Grande do Sul (UFRGS)
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionUMC
dc.date.accessioned2014-05-27T11:19:35Z
dc.date.available2014-05-27T11:19:35Z
dc.date.issued1998-07-01
dc.description.abstractThe bridged sulphate complex [Pd2 (C2,dmba) (μ-SO4) (SO2)2] has been obtained by reacting a saturated solution of SO2 in methanol and the cyclometallated compound [Pd(C2,N-dmba)(μ-N3)]2; (dmba = N,N-dimethylbenzylamine), at room temperature for 24 h. Reaction product was characterized by elemental analysis, NMR comprising 13C{1H} and 1H nuclei and I.R. spectrum's measurements. Thermal behavior has been investigated and residual products identified by X-ray powder diffraction.en
dc.description.affiliationInstituto de Química UFRGS, Av. Bento Gonçalves, 9500, 91501-970 - Porto Alegre - RS
dc.description.affiliationInst. de Química de Ararquara UNESP, CP 355, 14801-970 - Araraquara - SP
dc.description.affiliationCentro de Ciências Exatas UMC, Av. Candido Xavier Al. Souza, 200, 08780-210 - Mogi das Cruzes - SP
dc.description.affiliationUnespInst. de Química de Ararquara UNESP, CP 355, 14801-970 - Araraquara - SP
dc.format.extent394-396
dc.identifierhttp://dx.doi.org/10.1590/S0100-40421998000400003
dc.identifier.citationQuimica Nova, v. 21, n. 4, p. 394-396, 1998.
dc.identifier.doi10.1590/S0100-40421998000400003
dc.identifier.file2-s2.0-3242808800.pdf
dc.identifier.issn0100-4042
dc.identifier.lattes3300223970814448
dc.identifier.scieloS0100-40421998000400003
dc.identifier.scopus2-s2.0-3242808800
dc.identifier.urihttp://hdl.handle.net/11449/65466
dc.identifier.wosWOS:000074730600002
dc.language.isoeng
dc.relation.ispartofQuímica Nova
dc.relation.ispartofjcr0.646
dc.relation.ispartofsjr0,255
dc.rights.accessRightsAcesso aberto
dc.sourceScopus
dc.subjectAzido-cyclopalladated
dc.subjectReactivity
dc.subjectSulphur dioxide
dc.subjectThermal decomposition
dc.titleSynthesis, characterization and thermal decomposition of [Pd2 (C2-dmba) (μ-SO4) (μ-SO4) SO22]en
dc.typeArtigo
dcterms.licensehttp://www.scielo.br/revistas/qn/paboutj.htm#03
dspace.entity.typePublication
unesp.author.lattes3300223970814448[2]
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
unesp.departmentQuímica Inorgânica - IQARpt

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