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Effect of ceria content on the sintering of ZrO2 based ceramics synthesized from a polymeric precursor

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dc.contributor.authorQuinelato, A. L.
dc.contributor.authorLongo, Elson [UNESP]
dc.contributor.authorPerazolli, Leining Antonio [UNESP]
dc.contributor.authorVarela, José Arana [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionComiss Nacl Energie Nucl
dc.contributor.institutionUniversidade Federal de São Carlos (UFSCar)
dc.date.accessioned2014-05-20T15:23:59Z
dc.date.available2014-05-20T15:23:59Z
dc.date.issued2000-07-01
dc.description.abstractZirconia-ceria powders with ceria concentration varying from 0 to 12 mol% were synthesized using a polymeric precursor route based on the Pechini process. Powder characteristics were evaluated with regard to the crystallite size, BET surface area, phase distribution, nitrogen adsorption/desorption behavior, and agglomeration state. Sintering was studied considering the shrinkage rate, densification, grain size, and phase evolution. It was demonstrated that the synthesis method is effective to prepare nanosized powders of tetragonal zirconia single-phase. Sinterability mainly depended on the agglomeration state of powders and the monoclinic phase content, fully tetragonal zirconia ceramic, with grain size of 2.4 mu m, was obtained after addition of at least 9 mol% ceria and sintering at 1500 degrees C for 4 h. (C) 2000 Elsevier B.V. Ltd. All rights reserved.en
dc.description.affiliationUniv Estadual Paulista, Inst Quim, São Paulo, Brazil
dc.description.affiliationComiss Nacl Energie Nucl, Pocos de Caldas, Brazil
dc.description.affiliationUniv Fed Sao Carlos, Dept Quim, BR-13560 Sao Carlos, SP, Brazil
dc.description.affiliationUnespUniv Estadual Paulista, Inst Quim, São Paulo, Brazil
dc.format.extent1077-1084
dc.identifierhttp://dx.doi.org/10.1016/S0955-2219(99)00269-1
dc.identifier.citationJournal of the European Ceramic Society. Oxford: Elsevier B.V., v. 20, n. 8, p. 1077-1084, 2000.
dc.identifier.doi10.1016/S0955-2219(99)00269-1
dc.identifier.issn0955-2219
dc.identifier.lattes3822723627284619
dc.identifier.orcid0000-0003-1153-2742
dc.identifier.urihttp://hdl.handle.net/11449/34651
dc.identifier.wosWOS:000087098100008
dc.language.isoeng
dc.publisherElsevier B.V.
dc.relation.ispartofJournal of the European Ceramic Society
dc.relation.ispartofjcr3.794
dc.relation.ispartofsjr1,068
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectCeO2pt
dc.subjectmicrostructure-finalpt
dc.subjectpowders-chemical preparationpt
dc.subjectprecursors-organicpt
dc.subjectsinteringpt
dc.subjectZrO2pt
dc.titleEffect of ceria content on the sintering of ZrO2 based ceramics synthesized from a polymeric precursoren
dc.typeArtigo
dcterms.licensehttp://www.elsevier.com/about/open-access/open-access-policies/article-posting-policy
dcterms.rightsHolderElsevier B.V.
dspace.entity.typePublication
unesp.author.lattes3822723627284619[3]
unesp.author.orcid0000-0003-1153-2742[3]
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
unesp.departmentBioquímica e Tecnologia - IQARpt
unesp.departmentFísico-Química - IQARpt

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Araraquara - IQAR - Instituto de Química