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New layered double hydroxides intercalated with substituted pyrroles. 1. In situ polymerization of 4-(1H-pyrrol-1-yl)benzoate

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dc.contributor.authorTronto, Jairo
dc.contributor.authorLeroux, Fabrice
dc.contributor.authorCrepaldi, Eduardo Luis
dc.contributor.authorNaal, Zeki
dc.contributor.authorKlein, Stanlei Ivair [UNESP]
dc.contributor.authorValim, Joao Barros
dc.contributor.institutionUniversidade de São Paulo (USP)
dc.contributor.institutionUniv Clermont Ferrand
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2014-05-20T15:21:03Z
dc.date.available2014-05-20T15:21:03Z
dc.date.issued2006-05-01
dc.description.abstractThe two-dimensional hybrid organic-inorganic materials Zn-2-Cr and Zn-2-Al-LDHs (Layered Double Hydroxides) containing 4-(1H-pyrrol-1yl)benzoate anions as the interlayer anions were synthesized by the co-precipitation method at constant pH followed by subsequent hydrothermal treatment for 72 h. The materials were characterized by PXRD, C-13 CP-MAS NMR, ESR, TGA, and TEM. The basal spacing found by the X-ray diffraction technique is coincident with the formation of bilayers of the intercalated anions. Solid-state C-13 NMR and ESR data strongly suggest the partial in situ polymerization of the 4-(1H-pyrrol-1yl)benzoate anions during coprecipitation. (c) 2006 Elsevier Ltd. All rights reserved.en
dc.description.affiliationUniv São Paulo, Fac Filosofia Ciências & Letras Ribeirao Pret, Dept Quim, BR-14040901 Ribeirao Preto, SP, Brazil
dc.description.affiliationUniv Clermont Ferrand, CNRS, UMR 6002, Lab Mat Inorgan, F-63177 Clermont Ferrand, France
dc.description.affiliationUniv São Paulo, Fac Ciências Farmaceut Ribeirao Preto, Dept Quim & Fis, BR-14040903 Ribeirao Preto, SP, Brazil
dc.description.affiliationUniv Estadual Paulista, Inst Quim Araraquara, Dept Quim Inorgan, BR-1480090 Araraquara, SP, Brazil
dc.description.affiliationUnespUniv Estadual Paulista, Inst Quim Araraquara, Dept Quim Inorgan, BR-1480090 Araraquara, SP, Brazil
dc.format.extent968-972
dc.identifierhttp://dx.doi.org/10.1016/j.jpcs.2006.01.012
dc.identifier.citationJournal of Physics and Chemistry of Solids. Oxford: Pergamon-Elsevier B.V., v. 67, n. 5-6, p. 968-972, 2006.
dc.identifier.doi10.1016/j.jpcs.2006.01.012
dc.identifier.issn0022-3697
dc.identifier.lattes2545904877423127
dc.identifier.urihttp://hdl.handle.net/11449/32236
dc.identifier.wosWOS:000239261500016
dc.language.isoeng
dc.publisherElsevier B.V.
dc.relation.ispartofJournal of Physics and Chemistry of Solids
dc.relation.ispartofjcr2.207
dc.relation.ispartofsjr0,594
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectnanostructurespt
dc.subjectpolymerspt
dc.subjectX-ray diffractionpt
dc.subjectnuclear magnetic resonance (NMR)pt
dc.subjectelectron paramagnetic resonance (EPR)pt
dc.titleNew layered double hydroxides intercalated with substituted pyrroles. 1. In situ polymerization of 4-(1H-pyrrol-1-yl)benzoateen
dc.typeArtigo
dcterms.licensehttp://www.elsevier.com/about/open-access/open-access-policies/article-posting-policy
dcterms.rightsHolderElsevier B.V.
dspace.entity.typePublication
unesp.author.lattes2545904877423127
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
unesp.departmentQuímica Inorgânica - IQARpt

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Araraquara - IQAR - Instituto de Química