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Thermal decomposition of palladium(II) pyrazolyl complexes. Part I

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dc.contributor.authorNetto, AVG
dc.contributor.authorTakahashi, P. M.
dc.contributor.authorFrem, RCG
dc.contributor.authorMauro, Antonio Eduardo [UNESP]
dc.contributor.authorZorel, H. E.
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionFac Intergradas Catolicas Palmas
dc.date.accessioned2014-05-20T15:21:35Z
dc.date.available2014-05-20T15:21:35Z
dc.date.issued2004-08-01
dc.description.abstractThe thermal behavior of simple and mixed pyrazolyl complexes [PdCl2(phmPz)(2)] (1),[Pd(N-3)(2)(phmPz)(2)] (2), [Pd(SCN)(2)(phmPz)(2)] (3), and [Pd(N-3)(SCN)(phmPz)(2)] (4) (phmPz: 1-phenyl-3-methylpyrazole) has been investigated by means of thermogravimetry (TG) and differential thermal analysis (DTA). From the initial decomposition temperatures, the thermal stability of the complexes can be ordered in the sequence: 4 < 2 < 3 < 1. The final products of the thermal decompositions were characterized as metallic palladium (Pd-0). (C) 2004 Elsevier B.V. All rights reserved.en
dc.description.affiliationUNESP, Inst Quim, Dept Quim Geral & Inorgan, BR-14801970 Araraquara, SP, Brazil
dc.description.affiliationFac Intergradas Catolicas Palmas, Palmas, PR, Brazil
dc.description.affiliationUnespUNESP, Inst Quim, Dept Quim Geral & Inorgan, BR-14801970 Araraquara, SP, Brazil
dc.format.extent183-189
dc.identifierhttp://dx.doi.org/10.1016/j.jaap.2004.03.010
dc.identifier.citationJournal of Analytical and Applied Pyrolysis. Amsterdam: Elsevier B.V., v. 72, n. 1, p. 183-189, 2004.
dc.identifier.doi10.1016/j.jaap.2004.03.010
dc.identifier.issn0165-2370
dc.identifier.lattes3300223970814448
dc.identifier.lattes8534138813417161
dc.identifier.orcid0000-0003-1574-681X
dc.identifier.urihttp://hdl.handle.net/11449/32709
dc.identifier.wosWOS:000224009700020
dc.language.isoeng
dc.publisherElsevier B.V.
dc.relation.ispartofJournal of Analytical and Applied Pyrolysis
dc.relation.ispartofjcr3.468
dc.relation.ispartofsjr1,129
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectpalladiumpt
dc.subjectpyrazolespt
dc.subjectIR and NMR spectroscopypt
dc.subjectthermal analysispt
dc.titleThermal decomposition of palladium(II) pyrazolyl complexes. Part Ien
dc.typeArtigo
dcterms.licensehttp://www.elsevier.com/about/open-access/open-access-policies/article-posting-policy
dcterms.rightsHolderElsevier B.V.
dspace.entity.typePublication
unesp.author.lattes3300223970814448[4]
unesp.author.lattes8534138813417161[3]
unesp.author.orcid0000-0003-1574-681X[3]
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
unesp.departmentQuímica Inorgânica - IQARpt

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Araraquara - IQAR - Instituto de Química