Publicação: Characterization, and crystal structure of thiophenyl-2-methylidene-2- aminophenol
| dc.contributor.author | Cuin, A. | |
| dc.contributor.author | Pereira, G. A. | |
| dc.contributor.author | Bortoluzzi, A. J. | |
| dc.contributor.author | Massabni, Antonio Carlos [UNESP] | |
| dc.contributor.author | Corbi, P. P. | |
| dc.contributor.institution | Universidade Federal de Juiz de Fora (UFJF) | |
| dc.contributor.institution | Universidade Federal de Santa Catarina (UFSC) | |
| dc.contributor.institution | Universidade Estadual Paulista (Unesp) | |
| dc.contributor.institution | Universidade Estadual de Campinas (UNICAMP) | |
| dc.date.accessioned | 2014-05-27T11:28:20Z | |
| dc.date.available | 2014-05-27T11:28:20Z | |
| dc.date.issued | 2013-02-01 | |
| dc.description.abstract | The Schiff base thiophenyl-2-methylidene-2-aminophenol (ImineOH) is obtained from a stoichiometric mixture of 2-thiophenecarboxaldehyde and 2-aminophenol in ethanol under reflux at 90 C. Its crystal structure is determined by single crystal X-ray diffraction. ImineOH packs in an orthorhombic unit cell in the Pbca space group with the unit cell parameters a = 16.942(4) Å, b = 13.4395(11) Å, and c = 17.5857(12) Å, V = 4004.1(10) Å3, Z = 16. Strong hydrogen bonds are present in the ImineOH structure. Apart from the X-ray study, ImineOH was characterized by elemental analysis (CHN-S) and FT-IR (4000 cm-1 to 400 cm-1), UV-Vis and 13C, 1H, and 15N NMR spectroscopic measurements. © 2013 Pleiades Publishing, Ltd. | en |
| dc.description.affiliation | Chemistry Department Exact Sciences Institute UFJF Juiz de Fora, Fora, MG | |
| dc.description.affiliation | LABINC Chemistry Department UFSC Florianópolis, Florianópolis, SC | |
| dc.description.affiliation | Inorganic and General Chemistry Department Institute of Chemistry UNESP Araraquara, Araraquara, SP | |
| dc.description.affiliation | Institute of Chemistry Campinas State University UNICAMP Campinas, Campinas, SP | |
| dc.description.affiliationUnesp | Inorganic and General Chemistry Department Institute of Chemistry UNESP Araraquara, Araraquara, SP | |
| dc.format.extent | 269-273 | |
| dc.identifier | http://dx.doi.org/10.1134/S0022476613010423 | |
| dc.identifier.citation | Journal of Structural Chemistry, v. 54, n. 1, p. 269-273, 2013. | |
| dc.identifier.doi | 10.1134/S0022476613010423 | |
| dc.identifier.issn | 0022-4766 | |
| dc.identifier.scopus | 2-s2.0-84875656030 | |
| dc.identifier.uri | http://hdl.handle.net/11449/74520 | |
| dc.identifier.wos | WOS:000316757800042 | |
| dc.language.iso | eng | |
| dc.relation.ispartof | Journal of Structural Chemistry | |
| dc.relation.ispartofjcr | 0.521 | |
| dc.relation.ispartofsjr | 0,267 | |
| dc.rights.accessRights | Acesso restrito | pt |
| dc.source | Scopus | |
| dc.subject | 2-aminophenol | |
| dc.subject | 2-thiophenecarboxaldehyde | |
| dc.subject | Schiff base | |
| dc.subject | thiophenyl-2-methylidene-2-aminophenol | |
| dc.title | Characterization, and crystal structure of thiophenyl-2-methylidene-2- aminophenol | en |
| dc.type | Artigo | pt |
| dcterms.license | http://www.springer.com/open+access/authors+rights | |
| dspace.entity.type | Publication | |
| relation.isOrgUnitOfPublication | bc74a1ce-4c4c-4dad-8378-83962d76c4fd | |
| relation.isOrgUnitOfPublication.latestForDiscovery | bc74a1ce-4c4c-4dad-8378-83962d76c4fd | |
| unesp.campus | Universidade Estadual Paulista (UNESP), Instituto de Química, Araraquara | pt |
| unesp.department | Química Inorgânica - IQAR | pt |