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Characterization of amorphous niobium silicates powders synthesized by polymeric precursor method

dc.contributor.authorBertolini, M. J.
dc.contributor.authorZaghete, M. A.
dc.contributor.authorGimenes, R.
dc.contributor.authorPaiva-Santos, C. O.
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2014-05-20T15:20:20Z
dc.date.available2014-05-20T15:20:20Z
dc.date.issued2005-10-01
dc.description.abstractIn this paper 4.5SiO(2)-3Al(2)O(3-x)Nb(2)O(5)-2CaO powders have been synthesized using a chemical process the Polymeric Precursor Method. The process of glass formation has been investigated by XRD and DTA, the results confirm that the prepared powders are glasses. Experimental data show that amount of Nb2O5 had a considerable effect on the T-g values. The structures of glasses prepared. have been determined by Si-29 and Al-27 MAS NMR and the results indicated that the network is formed by SiO4 and AlO4 tetrahedral linked and probably Si-O-Nb bonds are present in the vitreous network. (C) 2005 Elsevier B.V. All rights reserved.en
dc.description.affiliationUNESP, Inst Quim, Ctr Multidisciplinar Desenvolvimento Mat Ceram, BR-14801970 São Paulo, Brazil
dc.description.affiliationUnespUNESP, Inst Quim, Ctr Multidisciplinar Desenvolvimento Mat Ceram, BR-14801970 São Paulo, Brazil
dc.format.extent3196-3199
dc.identifierhttp://dx.doi.org/10.1016/j.matlet.2005.04.054
dc.identifier.citationMaterials Letters. Amsterdam: Elsevier B.V., v. 59, n. 24-25, p. 3196-3199, 2005.
dc.identifier.doi10.1016/j.matlet.2005.04.054
dc.identifier.issn0167-577X
dc.identifier.urihttp://hdl.handle.net/11449/31664
dc.identifier.wosWOS:000231365800052
dc.language.isoeng
dc.publisherElsevier B.V.
dc.relation.ispartofMaterials Letters
dc.relation.ispartofjcr2.687
dc.rights.accessRightsAcesso restritopt
dc.sourceWeb of Science
dc.subjectniobiumpt
dc.subjectglassespt
dc.subjectpolymeric precursor methodpt
dc.titleCharacterization of amorphous niobium silicates powders synthesized by polymeric precursor methoden
dc.typeArtigopt
dcterms.licensehttp://www.elsevier.com/about/open-access/open-access-policies/article-posting-policy
dcterms.rightsHolderElsevier B.V.
dspace.entity.typePublication
relation.isOrgUnitOfPublicationbc74a1ce-4c4c-4dad-8378-83962d76c4fd
relation.isOrgUnitOfPublication.latestForDiscoverybc74a1ce-4c4c-4dad-8378-83962d76c4fd
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
unesp.departmentBioquímica e Tecnologia - IQpt

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