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Solid-state compounds of 2-methoxybenzylidenepyruvate with some bivalent metal ions - Synthesis, characterization and thermal behavior studies

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dc.contributor.authorKobelnik, M. [UNESP]
dc.contributor.authorSchnitzler, E.
dc.contributor.authorIonashiro, Massao [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionUniversidade Estadual de Ponta Grossa (UEPG)
dc.date.accessioned2014-05-20T15:29:59Z
dc.date.available2014-05-20T15:29:59Z
dc.date.issued2008-03-01
dc.description.abstractSolid-state M-2-MeO-BP compounds, where M represents bivalent Mn, Fe, Co, Ni, Cu, Zn and 2-MeO-BP is 2-methoxybenzylidenepyruvate have been synthesized. Simultaneous thermogravinietry-differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy, elemental analysis and complexometry were used to characterize and to study the thermal stability and thermal decomposition of these compounds. The results led to information about the composition, dehydration, crystallinity and thermal decomposition of the isolated compounds.en
dc.description.affiliationUniv Estadual Paulista, Inst Quim, BR-14801970 São Paulo, Brazil
dc.description.affiliationUniversidade Estadual de Ponta Grossa (UEPG), Dept Quim, Ponta Grossa, Parana, Brazil
dc.description.affiliationUnespUniv Estadual Paulista, Inst Quim, BR-14801970 São Paulo, Brazil
dc.format.extent891-895
dc.identifierhttp://dx.doi.org/10.1007/s10973-007-8505-x
dc.identifier.citationJournal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 91, n. 3, p. 891-895, 2008.
dc.identifier.doi10.1007/s10973-007-8505-x
dc.identifier.issn1388-6150
dc.identifier.lattes8460531302083773
dc.identifier.scopus2-s2.0-45449091549
dc.identifier.urihttp://hdl.handle.net/11449/132344
dc.identifier.wosWOS:000254522500033
dc.language.isoeng
dc.publisherSpringer
dc.relation.ispartofJournal of Thermal Analysis and Calorimetry
dc.relation.ispartofjcr2.209
dc.relation.ispartofsjr0,587
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subject2-methoxybenzylidenepyruvate
dc.subjectBivalent transition metals
dc.subjectCharacterization
dc.subjectThermal behavior
dc.subjectBackpropagation
dc.subjectChemical analysis
dc.subjectChemical modification
dc.subjectCobalt compounds
dc.subjectDecomposition
dc.subjectDifferential scanning calorimetry
dc.subjectGravimetric analysis
dc.subjectInfrared spectroscopy
dc.subjectIron
dc.subjectManganese
dc.subjectManganese compounds
dc.subjectMetal analysis
dc.subjectMetal ions
dc.subjectMixtures
dc.subjectNickel
dc.subjectPhotoresists
dc.subjectPyrolysis
dc.subjectScanning
dc.subjectSpectroscopic analysis
dc.subjectSpectroscopy
dc.subjectSpectrum analysis
dc.subjectTellurium compounds
dc.subjectThermoanalysis
dc.subjectThermogravimetric analysis
dc.subjectX ray analysis
dc.subjectX ray spectroscopy
dc.subjectZinc
dc.subject2 methoxybenzylidenepyruvate
dc.subjectBivalent metal ions
dc.subjectBusiness media
dc.subjectComplexometry
dc.subjectcrystallinity
dc.subjectDifferential scanning calorimetry (photo-DSC)
dc.subjectElemental analysis (EA)
dc.subjectInfrared (IR)
dc.subjectIsolated compounds
dc.subjectSolid-state compounds
dc.subjectSpringer (CO)
dc.subjectthermal stability
dc.subjectx-ray powder diffractometry
dc.subjectDifferential thermal analysis
dc.titleSolid-state compounds of 2-methoxybenzylidenepyruvate with some bivalent metal ions - Synthesis, characterization and thermal behavior studiesen
dc.typeArtigo
dcterms.licensehttp://www.springer.com/open+access/authors+rights?SGWID=0-176704-12-683201-0
dcterms.rightsHolderSpringer
dspace.entity.typePublication
unesp.author.lattes8460531302083773
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
unesp.departmentQuímica Analítica - IQARpt

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Araraquara - IQAR - Instituto de Química