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Fast and selective synthesis of mono-substituted sucrose methacrylate ester monomer

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dc.contributor.authorRojas Sterling, Juan Camilo
dc.contributor.authorOrtega, Julieth Orduña [UNESP]
dc.contributor.authorMetzker, Gustavo [UNESP]
dc.contributor.authorBoscolo, Mauricio [UNESP]
dc.contributor.authorMora Vargas, Jorge Andres [UNESP]
dc.contributor.institutionFacultad de Ciencias Básicas – Campus Pampalinda
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)
dc.date.accessioned2022-04-29T08:36:13Z
dc.date.available2022-04-29T08:36:13Z
dc.date.issued2022-01-01
dc.description.abstractSucrose methacrylate (SM) is a key monomer for synthesizing biocompatible polymers with a carbohydrate core. However, controlled SM synthesis is challenging due to the possible formation of regio-isomers. This study describes SM synthesis that involves ultrasound irradiation of a homogeneous basic medium. The selectivity for mono-substituted SM was 86% within 30 min of reaction. The newly developed methodology is faster and more selective than that of mono-substituted SM synthesis already described in the literature.en
dc.description.affiliationUniversidad Santiago de Cali (USC) Facultad de Ciencias Básicas – Campus Pampalinda
dc.description.affiliationSao Paulo State University (UNESP-IBILCE) Department of Chemistry and Environmental Sciences, Sao Jose Do Rio Preto
dc.description.affiliationUnespSao Paulo State University (UNESP-IBILCE) Department of Chemistry and Environmental Sciences, Sao Jose Do Rio Preto
dc.description.sponsorshipCoordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
dc.description.sponsorshipFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
dc.description.sponsorshipIdCAPES: 1760327
dc.description.sponsorshipIdFAPESP: 2013/23886–4
dc.description.sponsorshipIdFAPESP: 2017/13230–5
dc.description.sponsorshipIdFAPESP: 2020/02471-4
dc.identifierhttp://dx.doi.org/10.1016/j.carres.2021.108465
dc.identifier.citationCarbohydrate Research, v. 511.
dc.identifier.doi10.1016/j.carres.2021.108465
dc.identifier.issn1873-426X
dc.identifier.issn0008-6215
dc.identifier.scopus2-s2.0-85118591866
dc.identifier.urihttp://hdl.handle.net/11449/229843
dc.language.isoeng
dc.relation.ispartofCarbohydrate Research
dc.sourceScopus
dc.subjectMethacrylate
dc.subjectMonomer
dc.subjectSucrose ester
dc.subjectUltrasound
dc.titleFast and selective synthesis of mono-substituted sucrose methacrylate ester monomeren
dc.typeArtigo
dspace.entity.typePublication
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Biociências, Letras e Ciências Exatas, São José do Rio Pretopt
unesp.departmentQuímica e Ciências Ambientais - IBILCEpt

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São José do Rio Preto - IBILCE - Instituto de Biociências, Letras e Ciências Exatas