Publicação: Magnetic properties of spindle-type iron fine particles obtained from hematite
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Data
2001-12-01
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Spindle-type iron fine particles have been prepared by reduction of silica-coated-hematite particles. Hydrogen reduction of the coated-hematite cores yielded uniform spindle-type iron particles, which were stabilized by surface oxidation. Narrow particle distributions are observed from TEM measurements. X-ray, Mössbauer and magnetization data are in agreement with the presence of nanosized α-Fe particles, having surface layer of spinel structure oxide. Mössbauer spectra show that the oxide surface is superparamagnetic at room temperature. © 2001 Elsevier Science B.V. All rights reserved.
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Fine particles, Iron particles, Magnetic pigments, Magnetic recording media, Hematite particles, Hydrogen reduction, Iron-fines, Magnetization data, Mossbauer, Nano-sized, Oxide surface, Particle distributions, Room temperature, Silica-Coated, Spinel structure, Superparamagnetics, Surface layers, Surface oxidations, TEM, Hematite, Iron ores, Magnetic devices, Magnetic properties, Magnetic recording, Magnetism, Molybdenum oxide, Reaction kinetics, Silica, Superparamagnetism, Surface structure, Magnetic bubbles
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Inglês
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Journal of Magnetism and Magnetic Materials, v. 226-230, n. PART II, p. 1933-1935, 2001.