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Solid-state compounds of 2-chlorobenzylidenepyruvate with some bivalent metal ions - Synthesis, characterization and thermal behaviour

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dc.contributor.authorBannach, G.
dc.contributor.authorSiqueira, A. B.
dc.contributor.authorIonashiro, E. Y.
dc.contributor.authorRodrigues, E. C.
dc.contributor.authorIonashiro, Massao [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2014-05-20T15:22:59Z
dc.date.available2014-05-20T15:22:59Z
dc.date.issued2007-12-01
dc.description.abstractSolid-state M-2-Cl-BP, where M stands for Mn, Fe, Co, Ni, Cu, Zn and Pb and 2-Cl-BP is 2-chlorobenzylidenepyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), simultaneous thermogravimetry and differential thermal analysis (TG-DTA), X-ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, thermal stability and thermal decomposition of the isolated compounds.en
dc.description.affiliationUNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil
dc.description.affiliationUnespUNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil
dc.format.extent873-879
dc.identifierhttp://dx.doi.org/10.1007/s10973-005-7060-6
dc.identifier.citationJournal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 90, n. 3, p. 873-879, 2007.
dc.identifier.doi10.1007/s10973-005-7060-6
dc.identifier.issn1388-6150
dc.identifier.lattes8460531302083773
dc.identifier.urihttp://hdl.handle.net/11449/33862
dc.identifier.wosWOS:000251410000037
dc.language.isoeng
dc.publisherSpringer
dc.relation.ispartofJournal of Thermal Analysis and Calorimetry
dc.relation.ispartofjcr2.209
dc.relation.ispartofsjr0,587
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectbivalent metalspt
dc.subject2-chlorobenzylidenepyruvatept
dc.subjectcoordination sitespt
dc.subjectthermal behaviourpt
dc.titleSolid-state compounds of 2-chlorobenzylidenepyruvate with some bivalent metal ions - Synthesis, characterization and thermal behaviouren
dc.typeArtigo
dcterms.licensehttp://www.springer.com/open+access/authors+rights?SGWID=0-176704-12-683201-0
dcterms.rightsHolderSpringer
dspace.entity.typePublication
unesp.author.lattes8460531302083773
unesp.author.orcid0000-0002-8790-5069[1]
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
unesp.departmentQuímica Analítica - IQARpt

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Araraquara - IQAR - Instituto de Química