Effect of glazing application side and mechanical cycling on the biaxial flexural strength and Weibull characteristics of a Y-TZP ceramic
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2020-01-01
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Lobo, Carolina Machado Martinelli [UNESP]
Sacorague, Sâmia Carolina Mota Cavalcanti [UNESP]
Silva, Nathalia Ramos da
Costa, Anna Karina Figueiredo [UNESP]
Alves, Larissa Marcia Martins [UNESP]
Bottino, Marco Antônio [UNESP]
Özcan, Mutlu
Souza, Rodrigo Othávio de Assunção E
Melo, Renata Marques de [UNESP]
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OBJECTIVE: Glaze application on monolithic zirconia (Y-TZP) can be a practical approach to improve the mechanical properties of this material. Our study evaluated the effect of glazing side and mechanical cycling on the biaxial flexure strength (BFS) of a Y-TZP. METHODOLOGY: Eighty sintered Y-TZP discs (Ø:12 mm; thickness: 1.2 mm - ISO 6872) were produced and randomly assigned into eight groups (n=10), according to the factors glazing side (control - no glazing; GT - glaze on tensile side; GC - glaze on compression side; GTC - glaze on both sides) and mechanical aging (non-aged and aged, A - mechanical cycling: 1.2×106, 84 N, 3 Hz, under water at 37°C). Specimens were subjected to BFS test (1 mm/min; 1,000 Kgf load cell) and fractured surfaces were analyzed by stereomicroscopy and SEM. Hsueh's rigorous solutions were used to estimate the stress at failure of glazed specimens. Two-way ANOVA, Tukey's test (5%), and Weibull analysis were performed. RESULTS: The glazing side, mechanical aging and the interaction of the factors were significant (p<0.05). Groups GC (1157.9±146.9 MPa), GT (1156.1±195.3 MPa), GTC (986.0±187.4 MPa) and GTC-A (1131.9±128.9 MPa) presented higher BFS than control groups (Tukey, 5%). Hsueh's rigorous solutions showed that the maximum tensile stress was presented in the bottom of zirconia layer, at the zirconia/glaze interface. Weibull characteristic strength (σo) of the GC was higher than all groups (p<0.05), except to GT, GTC-A and GTC, which were similar among them. The fractography showed initiation of failures from zirconia the tensile side regardless of the side of glaze application and fatigue. CONCLUSION: Glazing zirconia applied on both tensile and compression sides improves the flexural strength of Y-TZP, regardless the mechanical aging.
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Journal of applied oral science : revista FOB, v. 28, p. e20200438-.