Hydrothermal treatment of gadolinium oxide in presence of silica

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dc.contributor.authorSimoneti, J. A. [UNESP]
dc.contributor.authorDavolos, Marian Rosaly [UNESP]
dc.contributor.authorJafelicci, M. [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2014-05-27T11:17:57Z
dc.date.available2014-05-27T11:17:57Z
dc.date.issued1994-12-01
dc.description.abstractHydrothermal and solvothermal (isopropanol) treatments of gadolinium oxide and silica were investigated under different pressure and temperature conditions. Products were examined by infrared vibrational spectroscopy (IR), x-ray powder diffraction (XRD) and thermal analysis (DTA, TG). Hexagonal gadolinium hydroxide was obtained in hydrothermal conditions, even in presence of silica, while no change was observed from isopropanolic medium treatment. Hydrothermally treated samples are more reactive as precursors for solid state reactions in inorganic synthesis.en
dc.description.affiliationUniversidade Estadual Paulista, Araraquara
dc.description.affiliationUnespUniversidade Estadual Paulista, Araraquara
dc.format.extent353-360
dc.identifierhttp://dx.doi.org/10.1080/08957959408201682
dc.identifier.citationHigh Pressure Research, v. 12, n. 4-6, p. 353-360, 1994.
dc.identifier.doi10.1080/08957959408201682
dc.identifier.issn0895-7959
dc.identifier.lattes4284809342546287
dc.identifier.scopus2-s2.0-0028736068
dc.identifier.urihttp://hdl.handle.net/11449/64517
dc.language.isoeng
dc.relation.ispartofHigh Pressure Research
dc.relation.ispartofjcr1.925
dc.relation.ispartofsjr0,690
dc.rights.accessRightsAcesso restrito
dc.sourceScopus
dc.subjectGadolinium compounds
dc.subjectHigh pressure effects
dc.subjectHigh temperature effects
dc.subjectOxides
dc.subjectPhase transitions
dc.subjectSilica
dc.subjectSingle crystals
dc.subjectSpectroscopy
dc.subjectThermal effects
dc.subjectThermoanalysis
dc.subjectX ray powder diffraction
dc.subjectGadolinium oxide
dc.subjectHexagonal gadolinium hydroxide
dc.subjectHydrothermal treatment
dc.subjectInfrared vibrational spectroscopy
dc.subjectIsopropanolic medium treatment
dc.subjectSolvothermal treatment
dc.subjectHeat treatment
dc.titleHydrothermal treatment of gadolinium oxide in presence of silicaen
dc.typeArtigo
unesp.author.lattes4284809342546287
unesp.author.orcid0000-0001-8326-1465[2]
unesp.campusUniversidade Estadual Paulista (Unesp), Instituto de Química, Araraquarapt

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