Study of the thermal behavior of Al(III) and In(III)-diclofenac complexes in solid state

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dc.contributor.authorKobelnik, Marcelo [UNESP]
dc.contributor.authorCassimiro, Douglas Lopes [UNESP]
dc.contributor.authorde Almeida, Adelia Emilia [UNESP]
dc.contributor.authorRibeiro, Clovis Augusto [UNESP]
dc.contributor.authorCrespi, Marisa Spirandeli [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionCtr Univ Norte Paulista UNORP
dc.date.accessioned2014-05-20T14:19:17Z
dc.date.available2014-05-20T14:19:17Z
dc.date.issued2011-08-01
dc.description.abstractThe Al and In-diclofenac compounds were prepared. Thermogravimetry (TG) and X-ray diffraction powder patterns were used to characterize these compounds. Details concerning the dehydration and thermal decomposition as well as data of kinetic parameters have been described here. The kinetic studies of these stages were evaluated from several heating rates with mass sample of 2 and 5 mg in open crucibles under nitrogen atmosphere. The results of the present study improve the knowledge on these compounds including their dehydration and thermal stability. The obtained data leads to a dependence on the sample mass, which results in two kinetic behavior patterns.en
dc.description.affiliationSão Paulo State Univ, Fac Ciencias Farmaceut, São Paulo, Brazil
dc.description.affiliationCtr Univ Norte Paulista UNORP, Sao Jose do Rio Preto, SP, Brazil
dc.description.affiliationSão Paulo State Univ, Inst Biociencias Letras & Ciencias Exatas, Sao Jose do Rio Preto, SP, Brazil
dc.description.affiliationSão Paulo State Univ, Inst Quim, BR-14800900 Araraquara, SP, Brazil
dc.description.affiliationUnespSão Paulo State Univ, Fac Ciencias Farmaceut, São Paulo, Brazil
dc.description.affiliationUnespSão Paulo State Univ, Inst Biociencias Letras & Ciencias Exatas, Sao Jose do Rio Preto, SP, Brazil
dc.description.affiliationUnespSão Paulo State Univ, Inst Quim, BR-14800900 Araraquara, SP, Brazil
dc.format.extent415-419
dc.identifierhttp://dx.doi.org/10.1007/s10973-010-1266-y
dc.identifier.citationJournal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 105, n. 2, p. 415-419, 2011.
dc.identifier.doi10.1007/s10973-010-1266-y
dc.identifier.issn1388-6150
dc.identifier.lattes8498310891810082
dc.identifier.lattes7471310113999140
dc.identifier.orcid0000-0002-7984-5908
dc.identifier.urihttp://hdl.handle.net/11449/25819
dc.identifier.wosWOS:000293213000005
dc.language.isoeng
dc.publisherSpringer
dc.relation.ispartofJournal of Thermal Analysis and Calorimetry
dc.relation.ispartofjcr2.209
dc.relation.ispartofsjr0,587
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectDiclofenacen
dc.subjectDehydrationen
dc.subjectThermal decompositionen
dc.subjectKinetic parametersen
dc.titleStudy of the thermal behavior of Al(III) and In(III)-diclofenac complexes in solid stateen
dc.typeArtigo
dcterms.licensehttp://www.springer.com/open+access/authors+rights?SGWID=0-176704-12-683201-0
dcterms.rightsHolderSpringer
unesp.author.lattes7471310113999140
unesp.author.lattes8498310891810082[4]
unesp.author.orcid0000-0002-7984-5908[4]
unesp.campusUniversidade Estadual Paulista (Unesp), Instituto de Química, Araraquarapt

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Artigos - Química Analítica - IQ