Synthesis, characterization and thermal behaviour of solid 4-methoxybenzoates of heavier trivalent lanthanides

dc.contributor.authorRodrigues, Emanuel C.
dc.contributor.authorSiqueira, Adriano B.
dc.contributor.authorIonashiro, Elias Y.
dc.contributor.authorBannach, Gilbert
dc.contributor.authorIonashiro, Massao [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2014-05-20T15:27:26Z
dc.date.available2014-05-20T15:27:26Z
dc.date.issued2006-12-01
dc.description.abstractSolid-state Ln-4-MeO-Bz compounds, where Ln stands for trivalent Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu and Y and 4-MeO-Bz is 4-methoxybenzoate, have been synthesized. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, phase transition, coordination mode, structure, thermal behaviour and thermal decomposition of the isolated compounds. The phase transition observed in the some compounds has been reported for the first time. (C) 2006 Elsevier B.V. All rights reserved.en
dc.description.affiliationUNESP, Inst Quim, BR-14801970 Araraquarra, SP, Brazil
dc.description.affiliationUnespUNESP, Inst Quim, BR-14801970 Araraquarra, SP, Brazil
dc.format.extent149-155
dc.identifierhttp://dx.doi.org/10.1016/j.tca.2006.09.014
dc.identifier.citationThermochimica Acta. Amsterdam: Elsevier B.V., v. 451, n. 1-2, p. 149-155, 2006.
dc.identifier.doi10.1016/j.tca.2006.09.014
dc.identifier.issn0040-6031
dc.identifier.lattes8460531302083773
dc.identifier.urihttp://hdl.handle.net/11449/37422
dc.identifier.wosWOS:000243142900022
dc.language.isoeng
dc.publisherElsevier B.V.
dc.relation.ispartofThermochimica Acta
dc.relation.ispartofjcr2.189
dc.relation.ispartofsjr0,605
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectheavier lanthanidespt
dc.subject4-methoxybenzoatept
dc.subjectcharacterizationpt
dc.subjectthermal behaviourpt
dc.titleSynthesis, characterization and thermal behaviour of solid 4-methoxybenzoates of heavier trivalent lanthanidesen
dc.typeArtigo
dcterms.licensehttp://www.elsevier.com/about/open-access/open-access-policies/article-posting-policy
dcterms.rightsHolderElsevier B.V.
unesp.author.lattes8460531302083773
unesp.author.orcid0000-0002-8790-5069[4]
unesp.campusUniversidade Estadual Paulista (Unesp), Instituto de Química, Araraquarapt

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