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Synthesis, characterization and thermal behaviour of heavy lanthanide and yttrium pyruvates in the solid state

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dc.contributor.authorSiqueira, A. B.
dc.contributor.authorde Carvalho, C. T. [UNESP]
dc.contributor.authorRodrigues, E. C.
dc.contributor.authorIonashiro, E. Y. [UNESP]
dc.contributor.authorBannach, Gilbert [UNESP]
dc.contributor.authorIonashiro, M.
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionFundação Educ Barretos
dc.contributor.institutionUniversidade Federal de Goiás (UFG)
dc.contributor.institutionUniversidade Federal de Mato Grosso (UFMT)
dc.date.accessioned2014-05-20T15:33:38Z
dc.date.available2014-05-20T15:33:38Z
dc.date.issued2010-04-01
dc.description.abstractSolid-state Ln-L compounds, where Ln stands for heavy trivalent lanthanides or yttrium (III) (Tb-Lu, Y) and where L is pyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), differential scanning calorimetry (DSC), X-Ray powder diffractometry, infrared spectroscopy, elemental analysis and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, thermal behaviour, ligand denticity of the isolated complexes.en
dc.description.affiliationUNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil
dc.description.affiliationFundação Educ Barretos, BR-14780000 Barretos, SP, Brazil
dc.description.affiliationUniversidade Federal de Goiás (UFG), Inst Quim, BR-74001979 Goiania, Go, Brazil
dc.description.affiliationUNESP, Fac Ciencias Bauru, BR-17033360 Bauru, Brazil
dc.description.affiliationUFMT, Inst Ciencias Exatas & Terra, BR-78698000 Pontal do Araguaia, MT, Brazil
dc.description.affiliationUnespUNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil
dc.description.affiliationUnespUNESP, Fac Ciencias Bauru, BR-17033360 Bauru, Brazil
dc.description.sponsorshipFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
dc.description.sponsorshipConselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
dc.description.sponsorshipCoordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
dc.description.sponsorshipIdFAPESP: 90/2932-4
dc.description.sponsorshipIdFAPESP: 05/00926-4
dc.format.extent95-100
dc.identifierhttp://dx.doi.org/10.1007/s10973-009-0537-y
dc.identifier.citationJournal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 100, n. 1, p. 95-100, 2010.
dc.identifier.doi10.1007/s10973-009-0537-y
dc.identifier.issn1388-6150
dc.identifier.urihttp://hdl.handle.net/11449/42201
dc.identifier.wosWOS:000276744500014
dc.language.isoeng
dc.publisherSpringer
dc.relation.ispartofJournal of Thermal Analysis and Calorimetry
dc.relation.ispartofjcr2.209
dc.relation.ispartofsjr0,587
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectHeavy lanthanides and yttriumen
dc.subjectPyruvateen
dc.subjectCharacterizationen
dc.subjectThermal behaviouren
dc.titleSynthesis, characterization and thermal behaviour of heavy lanthanide and yttrium pyruvates in the solid stateen
dc.typeArtigo
dcterms.licensehttp://www.springer.com/open+access/authors+rights?SGWID=0-176704-12-683201-0
dcterms.rightsHolderSpringer
dspace.entity.typePublication
unesp.author.orcid0000-0002-8790-5069[5]
unesp.campusUniversidade Estadual Paulista (UNESP), Faculdade de Ciências, Baurupt
unesp.departmentQuímica - FCpt

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