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On line extraction and separation of bendiocarb, methomyl, methylparathion, and pentachlorophenol pesticides from raw milk

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dc.contributor.authorMenezes, Manoel Lima de [UNESP]
dc.contributor.authorFelix, G.
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionENSCPB
dc.date.accessioned2014-05-20T13:26:46Z
dc.date.available2014-05-20T13:26:46Z
dc.date.issued1998-01-01
dc.description.abstractA high performance liquid chromatography (HPLC) method for extraction and determination of pesticides from raw milk was developed. The method involves direct injection of raw milk samples on a bovine serum albumin-dimethyl-octyl-silica gel (BSA-Si-Cs) column. The mobile phase 0.05 mol.L-1 phosphate buffer pH6.0 in acetonitrile (70:30 v/v) was employed for extraction and separation of bendiocarb, methylparathion, pentachlorophenol, and methomyl pesticides. The method shows good results of recovery in the pesticides studied, higher than 99.6%.en
dc.description.affiliationUniv Estadual Paulista, Fac Ciências, Dept Quim, BR-17033360 Bauru, SP, Brazil
dc.description.affiliationENSCPB, Chim Organ & Organomet Lab, CNRS, URA 35, F-33402 Talence, France
dc.description.affiliationUnespUniv Estadual Paulista, Fac Ciências, Dept Quim, BR-17033360 Bauru, SP, Brazil
dc.format.extent2863-2871
dc.identifierhttp://dx.doi.org/10.1080/10826079808003449
dc.identifier.citationJournal of Liquid Chromatography & Related Technologies. New York: Marcel Dekker Inc., v. 21, n. 18, p. 2863-2871, 1998.
dc.identifier.doi10.1080/10826079808003449
dc.identifier.issn1082-6076
dc.identifier.lattes4659698040759224
dc.identifier.urihttp://hdl.handle.net/11449/8668
dc.identifier.wosWOS:000076514500010
dc.language.isoeng
dc.publisherMarcel Dekker Inc
dc.relation.ispartofJournal of Liquid Chromatography & Related Technologies
dc.relation.ispartofjcr0.827
dc.relation.ispartofsjr0,297
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.titleOn line extraction and separation of bendiocarb, methomyl, methylparathion, and pentachlorophenol pesticides from raw milken
dc.typeArtigo
dcterms.licensehttp://journalauthors.tandf.co.uk/permissions/reusingOwnWork.asp
dcterms.rightsHolderMarcel Dekker Inc
dspace.entity.typePublication
unesp.author.lattes4659698040759224
unesp.campusUniversidade Estadual Paulista (UNESP), Faculdade de Ciências, Baurupt
unesp.departmentQuímica - FCpt

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