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Quantification of sex pheromone from Anocentor nitens by gas chromatography-mass spectrometry-selected ion monitoring

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dc.contributor.authorRodrigues, Clenilson M. [UNESP]
dc.contributor.authorBorges, Lígia M.F.
dc.contributor.authorFerri, Pedro H.
dc.contributor.authorFaria, Lourival C.
dc.contributor.institutionUniversidade Federal de Goiás (UFG)
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2014-05-27T11:21:02Z
dc.date.available2014-05-27T11:21:02Z
dc.date.issued2004-02-27
dc.description.abstractTwo highly sensitive and selective methods based on gas chromatography coupled to mass spectrometry (GC-MS) in the selected ion monitoring (SIM) mode have been developed for the quantification of 2,6-dichlorophenol (2,6-DCP), a sex pheromone of the tick females of Anocentor nitens. Standard addition method and calibration curve techniques using 5-bromine-4-hydroxy-3- methoxybenzaldehyde (5-BrV) as internal standard (IS) afforded detection limit of 0.1ngml-1. The calibration curve was linear over the concentration range from 0.5 to 500ngml-1 for 2,6-DCP. Results show that the concentration range of sex pheromone in the extracts samples was 1.08-10.35ngml-1. The methods developed provided reliable procedures to determine amounts of 2,6-DCP present in ticks. © 2003 Elsevier B.V. All rights reserved.en
dc.description.affiliationInstituto de Química Universidade Federal de Goiás, C.P. 131, 74001-970 Goiânia, GO
dc.description.affiliationDepartamento de Parasitologia Escola de Veterinária Universidade Federal de Goiás, C.P. 131, 74001-970 Goiânia, GO
dc.description.affiliationInstituto de Quimica UNESP, Av. Alberto Toloi, 185 Res. Marin., 14800105 Araraquara
dc.description.affiliationUnespInstituto de Quimica UNESP, Av. Alberto Toloi, 185 Res. Marin., 14800105 Araraquara
dc.format.extent637-641
dc.identifierhttp://dx.doi.org/10.1016/j.talanta.2003.09.009
dc.identifier.citationTalanta, v. 62, n. 3, p. 637-641, 2004.
dc.identifier.doi10.1016/j.talanta.2003.09.009
dc.identifier.issn0039-9140
dc.identifier.scopus2-s2.0-1042275790
dc.identifier.urihttp://hdl.handle.net/11449/67661
dc.language.isoeng
dc.relation.ispartofTalanta
dc.relation.ispartofjcr4.244
dc.relation.ispartofsjr1,186
dc.rights.accessRightsAcesso restritopt
dc.sourceScopus
dc.subject2,6-Dichlorophenol
dc.subjectAnocentor nitens
dc.subjectGC-MS-SIM
dc.subjectCalibration
dc.subjectGas chromatography
dc.subjectMass spectrometry
dc.subjectDetection limits
dc.subjectPhenols
dc.subject2,6 dichlorophenol
dc.subject5 bromine 4 hydroxy 3 methoxybenzaldehyde
dc.subjectbenzaldehyde derivative
dc.subjectsex pheromone
dc.subjectunclassified drug
dc.subjectcalibration
dc.subjectcontrolled study
dc.subjectextraction
dc.subjectfemale
dc.subjectgas chromatography
dc.subjecthormone determination
dc.subjection monitoring
dc.subjectmass spectrometry
dc.subjectnonhuman
dc.subjectquantitative analysis
dc.subjectsex difference
dc.subjectstandard
dc.subjecttechnique
dc.subjecttick
dc.titleQuantification of sex pheromone from Anocentor nitens by gas chromatography-mass spectrometry-selected ion monitoringen
dc.typeArtigopt
dcterms.licensehttp://www.elsevier.com/about/open-access/open-access-policies/article-posting-policy
dspace.entity.typePublication
relation.isOrgUnitOfPublicationbc74a1ce-4c4c-4dad-8378-83962d76c4fd
relation.isOrgUnitOfPublication.latestForDiscoverybc74a1ce-4c4c-4dad-8378-83962d76c4fd
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt

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Araraquara - IQAR - Instituto de Química