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Publicação:
Structure and absolute configuration of diterpenoids from hymenaea stigonocarpa

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dc.contributor.authorMonteiro, Afif F.
dc.contributor.authorBatista, Joao M. [UNESP]
dc.contributor.authorMachado, Michelle A.
dc.contributor.authorSeverino, Richele P.
dc.contributor.authorBlanch, Ewan W.
dc.contributor.authorBolzani, Vanderlan da Silva [UNESP]
dc.contributor.authorVieira, Paulo C.
dc.contributor.authorSeverino, Vanessa G. P.
dc.contributor.institutionUniversidade Federal de Goiás (UFG)
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionUniv Manchester
dc.contributor.institutionUniversidade Federal de São Carlos (UFSCar)
dc.date.accessioned2015-10-21T20:24:49Z
dc.date.available2015-10-21T20:24:49Z
dc.date.issued2015-06-01
dc.description.abstractChemical investigations of the ethanolic extracts from the flowers and leaves of Hymenaea stigonocarpa Mart. ex Hayne afforded one new ent-halimane diterpenoid, 18-hydroxy-ent-halima-1(10),13-(E)-dien-15-oic acid (1), together with five known compounds (2-6). The structural elucidation was performed by means of NMR (COSY, HSQC, HMBC, and NOESY) and MS analyses. Complete ¹H and ¹³C NMR data assignments are also reported for labd-13-en-8 beta-ol-15-oic (2) and labd-7,13-dien-15-oic (3) acids. The absolute configurations of 1 and 2 were established by comparison of experimental and calculated Raman optical activity spectra.en
dc.description.affiliationUniversidade Federal de Goiás (UFG), Unidade Acadêmica Especial de Física e Química, BR-75704020 Catalão, GO, Brasil
dc.description.affiliationUniversidade Estadual Paulista (UNESP), Instituto de Química (IQ), Departamento de Química Orgânica, BR-14800060 Araraquara, SP, Brasil
dc.description.affiliationUniv Manchester, Manchester Inst Biotechnol, Manchester M1 7DN, Lancs, England
dc.description.affiliationUniv Manchester, Fac Life Sci, Manchester M1 7DN, Lancs, England
dc.description.affiliationUniversidade Federal de São Carlos (UFSCar), Departamento de Química, BR-13565905 São Carlos, SP, Brasil
dc.description.affiliationUnespUniversidade Estadual Paulista (UNESP), Instituto de Química (IQ), Departamento de Química Orgânica, BR-14800060 Araraquara, SP, Brasil
dc.description.sponsorshipConselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
dc.description.sponsorshipCoordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
dc.description.sponsorshipFoundation for Research Support of the State of Goias (FAPEG)
dc.description.sponsorshipFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
dc.description.sponsorshipIdCNPq: 563286/2010-5
dc.description.sponsorshipIdFAPESP: 2010/52326-9
dc.description.sponsorshipIdFAPESP: 2013/07600-3
dc.description.sponsorshipIdFAPESP: 2014/50304-9
dc.format.extent1451-1455
dc.identifierhttp://pubs.acs.org/doi/abs/10.1021/acs.jnatprod.5b00166
dc.identifier.citationJournal Of Natural Products. Washington: Amer Chemical Soc, v. 78, n. 6, p. 1451-1455, 2015.
dc.identifier.doi10.1021/acs.jnatprod.5b00166
dc.identifier.issn0163-3864
dc.identifier.lattes4484083685251673
dc.identifier.urihttp://hdl.handle.net/11449/129124
dc.identifier.wosWOS:000357138300036
dc.language.isoeng
dc.publisherAmer Chemical Soc
dc.relation.ispartofJournal Of Natural Products
dc.relation.ispartofjcr3.885
dc.relation.ispartofsjr1,368
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.titleStructure and absolute configuration of diterpenoids from hymenaea stigonocarpaen
dc.typeArtigo
dcterms.rightsHolderAmer Chemical Soc
dspace.entity.typePublication
unesp.author.lattes4484083685251673
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
unesp.departmentQuímica Orgânica - IQARpt

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Araraquara - IQAR - Instituto de Química