Publicação: Thermal studies on nickel(II) 4-iodopyrazole complexes
dc.contributor.author | Takahashi, P. M. | |
dc.contributor.author | Frem, Regina C. G. | |
dc.contributor.author | Netto, A. V. G. | |
dc.contributor.author | Mauro, A. E. | |
dc.contributor.author | Matos, J. R. | |
dc.contributor.institution | Universidade Estadual Paulista (Unesp) | |
dc.contributor.institution | Universidade de São Paulo (USP) | |
dc.date.accessioned | 2014-05-20T15:28:47Z | |
dc.date.available | 2014-05-20T15:28:47Z | |
dc.date.issued | 2007-03-01 | |
dc.description.abstract | This work describes the synthesis, IR and UV-Vis spectroscopic characterization as well the thermal behavior of the [NiCl2(HIPz)(4)]center dot C3H6O (1), [Ni(H2O)(2)(HIPz)(4)](NO3)(2) (2), [Ni(NCS)(2)(HIPz)(4)] (3) and [Ni(N-3)(2)(HIPz)(4)] (4) (HIPz = 4-iodopyrazole) pyrazolyl complexes. TG experiments reveal that the compounds 1-4 undergo thermal decomposition in three or four mass loss steps yielding NiO as final residue, which was identified by X-ray powder diffraction. | en |
dc.description.affiliation | UNESP, Inst Quim Araraquara, BR-14801970 Araraquara, SP, Brazil | |
dc.description.affiliation | Univ São Paulo, Inst Quim, São Paulo, Brazil | |
dc.description.affiliationUnesp | UNESP, Inst Quim Araraquara, BR-14801970 Araraquara, SP, Brazil | |
dc.format.extent | 797-800 | |
dc.identifier | http://dx.doi.org/10.1007/s10973-006-7865-y | |
dc.identifier.citation | Journal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 87, n. 3, p. 797-800, 2007. | |
dc.identifier.doi | 10.1007/s10973-006-7865-y | |
dc.identifier.issn | 1388-6150 | |
dc.identifier.lattes | 8534138813417161 | |
dc.identifier.orcid | 0000-0003-1574-681X | |
dc.identifier.uri | http://hdl.handle.net/11449/38531 | |
dc.identifier.wos | WOS:000244823700037 | |
dc.language.iso | eng | |
dc.publisher | Springer | |
dc.relation.ispartof | Journal of Thermal Analysis and Calorimetry | |
dc.relation.ispartofjcr | 2.209 | |
dc.relation.ispartofsjr | 0,587 | |
dc.rights.accessRights | Acesso restrito | pt |
dc.source | Web of Science | |
dc.subject | DSC | pt |
dc.subject | 4-iodopyrazole | pt |
dc.subject | nickel(II) | pt |
dc.subject | pseudohalides | pt |
dc.subject | TG | pt |
dc.title | Thermal studies on nickel(II) 4-iodopyrazole complexes | en |
dc.type | Artigo | pt |
dcterms.license | http://www.springer.com/open+access/authors+rights?SGWID=0-176704-12-683201-0 | |
dcterms.rightsHolder | Springer | |
dspace.entity.type | Publication | |
unesp.author.lattes | 3300223970814448[4] | |
unesp.author.lattes | 8534138813417161[2] | |
unesp.author.orcid | 0000-0002-0057-7964[3] | |
unesp.author.orcid | 0000-0002-1793-7735[5] | |
unesp.author.orcid | 0000-0003-1574-681X[2] | |
unesp.campus | Universidade Estadual Paulista (UNESP), Instituto de Química, Araraquara | pt |
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