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Thermal studies on solid 1,4-bis(3-carboxy-3-oxo-prop-1-enyl) benzene of lighter trivalent lanthanides

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dc.contributor.authorNunes, Ronaldo S. [UNESP]
dc.contributor.authorBannach, Gilbert [UNESP]
dc.contributor.authorLuiz, Jose M. [UNESP]
dc.contributor.authorCaires, Flavio J. [UNESP]
dc.contributor.authorCarvalho, Claudio T.
dc.contributor.authorIonashiro, Massao [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionUniversidade Federal da Grande Dourados (UFGD)
dc.date.accessioned2014-05-20T13:26:53Z
dc.date.available2014-05-20T13:26:53Z
dc.date.issued2011-11-01
dc.description.abstractSolid-state compounds of general formula Ln(2)L(3)center dot nH(2)O, where L represents 1,4-bis(3-carboxy-3-oxo-prop-1-enyl)benzene and Ln = La, Ce, Pr, Nd, Sm, were synthesized. Complexometric titrations with EDTA, thermogravimetry (TG), differential thermal analysis (DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, elemental analysis and infrared spectroscopy have been employed to characterize and to study the thermal behavior of these compounds in dynamic air atmosphere. The results led to information about the composition, dehydration, crystallinity, and thermal decomposition of the synthesized compounds.en
dc.description.affiliationUNESP, Fac Engn Guaratingueta, BR-12516410 Guaratingueta, SP, Brazil
dc.description.affiliationUNESP, Fac Ciencias, Dept Quim, BR-17033260 Bauru, SP, Brazil
dc.description.affiliationUNESP, Inst Quim Araraquara, BR-14800900 Araraquara, SP, Brazil
dc.description.affiliationFundação Univ Fed Grande Dourados, BR-79804970 Dourados, MS, Brazil
dc.description.affiliationUnespUNESP, Fac Engn Guaratingueta, BR-12516410 Guaratingueta, SP, Brazil
dc.description.affiliationUnespUNESP, Fac Ciencias, Dept Quim, BR-17033260 Bauru, SP, Brazil
dc.description.affiliationUnespUNESP, Inst Quim Araraquara, BR-14800900 Araraquara, SP, Brazil
dc.format.extent525-529
dc.identifierhttp://dx.doi.org/10.1007/s10973-010-1250-6
dc.identifier.citationJournal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 106, n. 2, p. 525-529, 2011.
dc.identifier.doi10.1007/s10973-010-1250-6
dc.identifier.issn1388-6150
dc.identifier.lattes8460531302083773
dc.identifier.urihttp://hdl.handle.net/11449/8732
dc.identifier.wosWOS:000296065100035
dc.language.isoeng
dc.publisherSpringer
dc.relation.ispartofJournal of Thermal Analysis and Calorimetry
dc.relation.ispartofjcr2.209
dc.relation.ispartofsjr0,587
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subject1,4-bis(3-carboxy-3-oxo-prop-1-enyl) benzeneen
dc.subjectLighter lanthanidesen
dc.subjectThermal behavioren
dc.titleThermal studies on solid 1,4-bis(3-carboxy-3-oxo-prop-1-enyl) benzene of lighter trivalent lanthanidesen
dc.typeArtigo
dcterms.licensehttp://www.springer.com/open+access/authors+rights?SGWID=0-176704-12-683201-0
dcterms.rightsHolderSpringer
dspace.entity.typePublication
unesp.author.lattes8460531302083773
unesp.author.orcid0000-0002-5001-5038[1]
unesp.author.orcid0000-0002-8790-5069[2]
unesp.campusUniversidade Estadual Paulista (UNESP), Faculdade de Ciências, Baurupt
unesp.departmentQuímica - FCpt

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Bauru - FC - Faculdade de Ciências