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Synthesis and characterization of the mer-[RuCl3(NO)(dppb)] isomer. X-ray structures of fac-[RuCl3(NO)(dppm)], cis-[RuCl2(dppm)2] and mer-[RuCl3(NO)(dppb)] [dppm=1,2-Bis(diphenylphosphino)methane and dppb=1,4-Bis(diphenylphosphino)butane]

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dc.contributor.authorBatista, Alzir A.
dc.contributor.authorPereira, Cid
dc.contributor.authorWohnrath, Karen [UNESP]
dc.contributor.authorQueiroz, Salete L.
dc.contributor.authorDe A. Santos, Regina H.
dc.contributor.authorDo P. Gambardella, Maria Teresa
dc.contributor.institutionUniversidade Federal de São Carlos (UFSCar)
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionUniversidade de São Paulo (USP)
dc.date.accessioned2014-05-27T11:19:44Z
dc.date.available2014-05-27T11:19:44Z
dc.date.issued1999-06-11
dc.description.abstractThe fac-[RuCl3(NO)(dppm)] (1) and cis-[RuCl2(dppm)2] (2) complexes were obtained with co-crystallization in the solid state from the reaction of RuCl3(NO) with the diphosphine in dichloromethane. mer-[RuCl3(NO)(dppb)] (3) was obtained from [RuCl3(dppb)(H2O)] by bubbling NO for 30 min in the same solvent. The crystal and molecular structures of these three compounds have been determined from X-ray studies. © Elsevier Science Ltd.en
dc.description.affiliationDepartamento de Química UFSCar, CP 676, 13.565-905, SP, São Carlos
dc.description.affiliationInst. de Química/UNESP-CP 355 14800-900, (SP), Araraquara
dc.description.affiliationInst. de Quim. de São Carlos USP, CP 780, 13560-250, SP, São Carlos
dc.description.affiliationUnespInst. de Química/UNESP-CP 355 14800-900, (SP), Araraquara
dc.format.extent2079-2083
dc.identifierhttp://dx.doi.org/10.1016/S0277-5387(99)00084-4
dc.identifier.citationPolyhedron, v. 18, n. 15, p. 2079-2083, 1999.
dc.identifier.doi10.1016/S0277-5387(99)00084-4
dc.identifier.issn0277-5387
dc.identifier.scopus2-s2.0-0000130862
dc.identifier.urihttp://hdl.handle.net/11449/65794
dc.identifier.wosWOS:000081794600011
dc.language.isoeng
dc.relation.ispartofPolyhedron
dc.relation.ispartofjcr2.067
dc.relation.ispartofsjr0,472
dc.rights.accessRightsAcesso restrito
dc.sourceScopus
dc.subjectComplexes, Biphosphinesen
dc.subjectIsomerismen
dc.subjectNitrosylen
dc.subjectRutheniumen
dc.subjectX-ray structureen
dc.titleSynthesis and characterization of the mer-[RuCl3(NO)(dppb)] isomer. X-ray structures of fac-[RuCl3(NO)(dppm)], cis-[RuCl2(dppm)2] and mer-[RuCl3(NO)(dppb)] [dppm=1,2-Bis(diphenylphosphino)methane and dppb=1,4-Bis(diphenylphosphino)butane]en
dc.typeArtigo
dcterms.licensehttp://www.elsevier.com/about/open-access/open-access-policies/article-posting-policy
dspace.entity.typePublication

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