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Synthesis, characterisation and thermal behaviour of solid state compounds of 4-methylbenzylidenepyruvate with some bivalent metal ions

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dc.contributor.authorPetroni, I. A.
dc.contributor.authorFertonani, F. L.
dc.contributor.authorMelios, C. B.
dc.contributor.authorIonashiro, Massao [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2014-05-20T15:28:09Z
dc.date.available2014-05-20T15:28:09Z
dc.date.issued2003-04-17
dc.description.abstractSolid state M-4-Me-BP compounds, where M stands for bivalent Mn, Fe, Co, Ni, Cu, Zn, Pb and 4-Me-BP is 4-methylbenzylidenepyruvate, have been synthesized. Simultaneous thermogravimetry-differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterise and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, thermal stability and thermal decomposition of the isolated complexes. (C) 2002 Elsevier B.V. B.V. All rights reserved.en
dc.description.affiliationUNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil
dc.description.affiliationUnespUNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil
dc.format.extent187-198
dc.identifierhttp://dx.doi.org/10.1016/S0040-6031(02)00498-7
dc.identifier.citationThermochimica Acta. Amsterdam: Elsevier B.V., v. 400, n. 1-2, p. 187-198, 2003.
dc.identifier.doi10.1016/S0040-6031(02)00498-7
dc.identifier.issn0040-6031
dc.identifier.lattes8460531302083773
dc.identifier.urihttp://hdl.handle.net/11449/38025
dc.identifier.wosWOS:000182494100020
dc.language.isoeng
dc.publisherElsevier B.V.
dc.relation.ispartofThermochimica Acta
dc.relation.ispartofjcr2.189
dc.relation.ispartofsjr0,605
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectbivalent metalspt
dc.subject4-methylbenzylidenepyruvatept
dc.subjectcoordination sitespt
dc.subjectthermal behaviourpt
dc.titleSynthesis, characterisation and thermal behaviour of solid state compounds of 4-methylbenzylidenepyruvate with some bivalent metal ionsen
dc.typeArtigo
dcterms.licensehttp://www.elsevier.com/about/open-access/open-access-policies/article-posting-policy
dcterms.rightsHolderElsevier B.V.
dspace.entity.typePublication
unesp.author.lattes8460531302083773
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
unesp.departmentQuímica Analítica - IQARpt

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Araraquara - IQAR - Instituto de Química