Publicação: Synthesis, characterization, and thermal behavior of palladium(II) coordination compounds containing isonicotinamide
Carregando...
Data
Orientador
Coorientador
Pós-graduação
Curso de graduação
Título da Revista
ISSN da Revista
Título de Volume
Editor
Springer
Tipo
Artigo
Direito de acesso
Acesso restrito
Resumo
Palladium(II) coordination compounds of general formula trans-[PdX(2)(isn)(2)], X = Cl(-) (1), N(3) (-) (2), SCN(-) (3), NCO(-) (4), isn = isonicotinamide; were synthesized and characterized in solid state by elemental analysis, infrared spectroscopy, and simultaneous TG-DTA. TG experiments reveal that the compounds 1-4 undergo thermal decomposition in three or four stages, yielding Pd(0) as final residue, according to calculus and identification by X-ray powder diffraction.
Descrição
Palavras-chave
Palladium(II), Isonicotinamide, TG-DTA, IR spectroscopy
Idioma
Inglês
Como citar
Journal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 106, n. 2, p. 375-378, 2011.
