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Synthesis, characterization, and thermal behavior of palladium(II) coordination compounds containing isonicotinamide

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dc.contributor.authorde Souza, Rodrigo A. [UNESP]
dc.contributor.authorMauro, Antonio Eduardo [UNESP]
dc.contributor.authorNetto, Adelino Vieira de Godoy [UNESP]
dc.contributor.authorda Cunha, Gislaine A. [UNESP]
dc.contributor.authorde Almeida, Eduardo T.
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionUniversidade Federal de Alfenas (UNIFAL)
dc.date.accessioned2014-05-20T14:20:08Z
dc.date.available2014-05-20T14:20:08Z
dc.date.issued2011-11-01
dc.description.abstractPalladium(II) coordination compounds of general formula trans-[PdX(2)(isn)(2)], X = Cl(-) (1), N(3) (-) (2), SCN(-) (3), NCO(-) (4), isn = isonicotinamide; were synthesized and characterized in solid state by elemental analysis, infrared spectroscopy, and simultaneous TG-DTA. TG experiments reveal that the compounds 1-4 undergo thermal decomposition in three or four stages, yielding Pd(0) as final residue, according to calculus and identification by X-ray powder diffraction.en
dc.description.affiliationUNESP Univ Estadual Paulista, Inst Quim Araraquara, BR-14800900 Araraquara, SP, Brazil
dc.description.affiliationUNIFAL Univ Fed Alfenas, Dept Ciencias Exatas, BR-37130000 Alfenas, MG, Brazil
dc.description.affiliationUnespUNESP Univ Estadual Paulista, Inst Quim Araraquara, BR-14800900 Araraquara, SP, Brazil
dc.format.extent375-378
dc.identifierhttp://dx.doi.org/10.1007/s10973-010-1216-8
dc.identifier.citationJournal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 106, n. 2, p. 375-378, 2011.
dc.identifier.doi10.1007/s10973-010-1216-8
dc.identifier.issn1388-6150
dc.identifier.lattes3300223970814448
dc.identifier.lattes7927677053650819
dc.identifier.orcid0000-0002-0057-7964
dc.identifier.urihttp://hdl.handle.net/11449/26047
dc.identifier.wosWOS:000296065100011
dc.language.isoeng
dc.publisherSpringer
dc.relation.ispartofJournal of Thermal Analysis and Calorimetry
dc.relation.ispartofjcr2.209
dc.relation.ispartofsjr0,587
dc.rights.accessRightsAcesso restritopt
dc.sourceWeb of Science
dc.subjectPalladium(II)en
dc.subjectIsonicotinamideen
dc.subjectTG-DTAen
dc.subjectIR spectroscopyen
dc.titleSynthesis, characterization, and thermal behavior of palladium(II) coordination compounds containing isonicotinamideen
dc.typeArtigopt
dcterms.licensehttp://www.springer.com/open+access/authors+rights?SGWID=0-176704-12-683201-0
dcterms.rightsHolderSpringer
dspace.entity.typePublication
relation.isOrgUnitOfPublicationbc74a1ce-4c4c-4dad-8378-83962d76c4fd
relation.isOrgUnitOfPublication.latestForDiscoverybc74a1ce-4c4c-4dad-8378-83962d76c4fd
unesp.author.lattes3300223970814448[2]
unesp.author.lattes7927677053650819[3]
unesp.author.orcid0000-0002-0057-7964[3]
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
unesp.departmentQuímica Inorgânica - IQARpt

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Araraquara - IQAR - Instituto de Química