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dc.contributor.authorBernardi, M. I. B.
dc.contributor.authorFeitosa, C. A. C.
dc.contributor.authorPaskocimas, C. A.
dc.contributor.authorLongo, Elson [UNESP]
dc.contributor.authorPaiva-Santos, C. O. [UNESP]
dc.identifier.citationCeramics International. Oxford: Elsevier B.V., v. 35, n. 1, p. 463-466, 2009.
dc.description.abstractAn extensive work for the study of SnO(2) samples doped with x-mol% of Sb (x = 0, 6, 10, 14 and 18) is reported. The materials were prepared by the polymeric precursor method (Pechini method), calcined for 4 h between 800 degrees C and 1200 degrees C. The Rietveld method with X-ray diffraction data (XRD) was used to analyze the unit cell dimensions, crystallite size and microstrain. It was observed the crystallite size increasing and decrease of the microstrain with the increase of the calcining temperature. The synthesis of tin oxide nanoparticles with high thermal stability against particle growth rate was achieved by doping SnO(2) particles with Sb(2)O(3). All the phases tend to have the same dimension when the temperature increases, although its values varies with x and reaches the maximum value when fired at 1100 degrees C. These variations seem to be an indication that the oxidation state of the antimony changes with the amount of Sb added to the material. (C) 2008 Elsevier Ltd and Techna Group S.r.l. All rights reserved.en
dc.description.sponsorshipFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
dc.description.sponsorshipConselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
dc.description.sponsorshipCoordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
dc.publisherElsevier B.V.
dc.relation.ispartofCeramics International
dc.sourceWeb of Science
dc.subjectPowders: chemical preparationen
dc.subjectElectron microscopyen
dc.subjectX-ray methodsen
dc.titleDevelopment of metal oxide nanoparticles by soft chemical methoden
dcterms.rightsHolderElsevier B.V.
dc.contributor.institutionUniversidade de São Paulo (USP)
dc.contributor.institutionUniversidade Federal do Maranhão (UFMA)
dc.contributor.institutionUniversidade Federal do Rio Grande do Norte (UFRN)
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)
dc.description.affiliationUSP, Inst Fis, Grp Crescimento Cristais & Mat Ceram, BR-13560970 São Carlos, SP, Brazil
dc.description.affiliationUniversidade Federal do Maranhão (UFMA), Ctr Tecnol, Dept Fis, BR-65085580 Sao Luis, Ma, Brazil
dc.description.affiliationUniversidade Federal do Rio Grande do Norte (UFRN), Dept Engn Mecan, BR-59072970 Natal, RN, Brazil
dc.description.affiliationUNESP, Inst Quim, CMDMC, BR-14800900 Araraquara, SP, Brazil
dc.description.affiliationUnespUNESP, Inst Quim, CMDMC, BR-14800900 Araraquara, SP, Brazil
dc.rights.accessRightsAcesso restrito
unesp.campusUniversidade Estadual Paulista (UNESP), Instituto de Química, Araraquarapt
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