Publicação: Synthesis of PbTiO3 by use of polymeric precursors
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Lead titanate powders were synthesized through the use of polymeric precursors according to the Pechini Process. The polymeric precursor was calcined at temperatures ranging from 300 to 600°C for 1 or 2 h. X-ray diffraction (XRD) showed that lead titanate crystallizes from the precursor at temperatures as low as 400°C. No intermediate carbonate phase was detected by Fourier transform infrared spectroscopy (FTIR) or by XRD. A powder with mean particle size of 150 nm was obtained after calcination of the precursor at 600°C for 1 h. © 1998 Elsevier Science B.V. All rights reserved.
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Lead titanate, Low temperature, PbTiO3, Pechini process, Polymeric precursor, Synthesis, Calcination, Crystallization, Ferroelectric materials, Fourier transform infrared spectroscopy, Powders, Synthesis (chemical), Thermal effects, X ray diffraction analysis, Polymeric precursors, Lead compounds
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Inglês
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Materials Letters, v. 37, n. 1-2, p. 1-5, 1998.
