Effect of furfuryl alcohol addition on the cure of furfuryl alcohol resin used in the glassy carbon manufacture

dc.contributor.authorGaefke, C. B.
dc.contributor.authorBotelho, E. C.
dc.contributor.authorFerreira, N. G.
dc.contributor.authorRezende, M. C.
dc.contributor.institutionCTA
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionInstituto Nacional de Pesquisas Espaciais (INPE)
dc.date.accessioned2014-05-20T15:20:31Z
dc.date.available2014-05-20T15:20:31Z
dc.date.issued2007-11-15
dc.description.abstractGlassy carbon can be manufactured practically without pores, named Monolithic Vitreous Carbon (MVC) or presenting up to 98% in transport pore volume, foam form, denominated Reticulated Vitreous Carbon (RVC). The glassy carbon processing is affected by some processing parameters, among them it can be cited the resin viscosity. The present work involves the optimization of RVC manufacture by monitoring the polyurethane (PU) foam impregnation with furfuryl alcohol resin with different viscosity values, which were obtained by dilution of the resin with different amounts of furfuryl alcohol. The resin samples used in the PU impregnation were characterized by thermal and rheological analyses. These results were correlated with scanning electron microscopy observations and compression test results of the impregnated polyurethane foam. The results show that the rheological behavior of the resin has significant influence on the polymerization step, affecting the homogeneity of impregnated foam and, consequently, its final properties, mainly the mechanical one. The impregnated foam prepared with the furfuryl alcohol resin diluted with 10% of furfuryl alcohol (eta = 11.4 Pa s) showed higher compression values (0.26 MPa). (c) 2007 Wiley Periodicals, Inc.en
dc.description.affiliationCTA, IAE, Div Mat, BR-12228904 Sao Jose Dos Campos, SP, Brazil
dc.description.affiliationCTA, Inst Tecnol Aeronaut, Dept Eng Aeronaut & Mecan, BR-12228900 Sao Jose Dos Campos, SP, Brazil
dc.description.affiliationSão Paulo State Univ, Dept Mat & Technol, BR-12228915 São Paulo, Brazil
dc.description.affiliationInst Nacl Pesquisas Espaciais, BR-12228915 Sao Jose dos Campos, Brazil
dc.description.affiliationUnespSão Paulo State Univ, Dept Mat & Technol, BR-12228915 São Paulo, Brazil
dc.format.extent2274-2281
dc.identifierhttp://dx.doi.org/10.1002/app.26938
dc.identifier.citationJournal of Applied Polymer Science. Hoboken: John Wiley & Sons Inc., v. 106, n. 4, p. 2274-2281, 2007.
dc.identifier.doi10.1002/app.26938
dc.identifier.issn0021-8995
dc.identifier.lattes4378078337343660
dc.identifier.orcid0000-0001-8338-4879
dc.identifier.urihttp://hdl.handle.net/11449/31803
dc.identifier.wosWOS:000249590700016
dc.language.isoeng
dc.publisherWiley-Blackwell
dc.relation.ispartofJournal of Applied Polymer Science
dc.relation.ispartofjcr1.901
dc.relation.ispartofsjr0,543
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectreticulated vitreous carbonpt
dc.subjectfurfuryl alcohol resinpt
dc.subjectthermal analysespt
dc.subjectrheological analysespt
dc.titleEffect of furfuryl alcohol addition on the cure of furfuryl alcohol resin used in the glassy carbon manufactureen
dc.typeArtigo
dcterms.licensehttp://olabout.wiley.com/WileyCDA/Section/id-406071.html
dcterms.rightsHolderWiley-Blackwell
unesp.author.lattes4378078337343660[2]
unesp.author.orcid0000-0001-8338-4879[2]

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