Quantification of sex pheromone from Anocentor nitens by gas chromatography-mass spectrometry-selected ion monitoring
dc.contributor.author | Rodrigues, Clenilson M. [UNESP] | |
dc.contributor.author | Borges, Lígia M.F. | |
dc.contributor.author | Ferri, Pedro H. | |
dc.contributor.author | Faria, Lourival C. | |
dc.contributor.institution | Universidade Federal de Goiás (UFG) | |
dc.contributor.institution | Universidade Estadual Paulista (Unesp) | |
dc.date.accessioned | 2014-05-27T11:21:02Z | |
dc.date.available | 2014-05-27T11:21:02Z | |
dc.date.issued | 2004-02-27 | |
dc.description.abstract | Two highly sensitive and selective methods based on gas chromatography coupled to mass spectrometry (GC-MS) in the selected ion monitoring (SIM) mode have been developed for the quantification of 2,6-dichlorophenol (2,6-DCP), a sex pheromone of the tick females of Anocentor nitens. Standard addition method and calibration curve techniques using 5-bromine-4-hydroxy-3- methoxybenzaldehyde (5-BrV) as internal standard (IS) afforded detection limit of 0.1ngml-1. The calibration curve was linear over the concentration range from 0.5 to 500ngml-1 for 2,6-DCP. Results show that the concentration range of sex pheromone in the extracts samples was 1.08-10.35ngml-1. The methods developed provided reliable procedures to determine amounts of 2,6-DCP present in ticks. © 2003 Elsevier B.V. All rights reserved. | en |
dc.description.affiliation | Instituto de Química Universidade Federal de Goiás, C.P. 131, 74001-970 Goiânia, GO | |
dc.description.affiliation | Departamento de Parasitologia Escola de Veterinária Universidade Federal de Goiás, C.P. 131, 74001-970 Goiânia, GO | |
dc.description.affiliation | Instituto de Quimica UNESP, Av. Alberto Toloi, 185 Res. Marin., 14800105 Araraquara | |
dc.description.affiliationUnesp | Instituto de Quimica UNESP, Av. Alberto Toloi, 185 Res. Marin., 14800105 Araraquara | |
dc.format.extent | 637-641 | |
dc.identifier | http://dx.doi.org/10.1016/j.talanta.2003.09.009 | |
dc.identifier.citation | Talanta, v. 62, n. 3, p. 637-641, 2004. | |
dc.identifier.doi | 10.1016/j.talanta.2003.09.009 | |
dc.identifier.issn | 0039-9140 | |
dc.identifier.scopus | 2-s2.0-1042275790 | |
dc.identifier.uri | http://hdl.handle.net/11449/67661 | |
dc.language.iso | eng | |
dc.relation.ispartof | Talanta | |
dc.relation.ispartofjcr | 4.244 | |
dc.relation.ispartofsjr | 1,186 | |
dc.rights.accessRights | Acesso restrito | |
dc.source | Scopus | |
dc.subject | 2,6-Dichlorophenol | |
dc.subject | Anocentor nitens | |
dc.subject | GC-MS-SIM | |
dc.subject | Calibration | |
dc.subject | Gas chromatography | |
dc.subject | Mass spectrometry | |
dc.subject | Detection limits | |
dc.subject | Phenols | |
dc.subject | 2,6 dichlorophenol | |
dc.subject | 5 bromine 4 hydroxy 3 methoxybenzaldehyde | |
dc.subject | benzaldehyde derivative | |
dc.subject | sex pheromone | |
dc.subject | unclassified drug | |
dc.subject | calibration | |
dc.subject | controlled study | |
dc.subject | extraction | |
dc.subject | female | |
dc.subject | gas chromatography | |
dc.subject | hormone determination | |
dc.subject | ion monitoring | |
dc.subject | mass spectrometry | |
dc.subject | nonhuman | |
dc.subject | quantitative analysis | |
dc.subject | sex difference | |
dc.subject | standard | |
dc.subject | technique | |
dc.subject | tick | |
dc.title | Quantification of sex pheromone from Anocentor nitens by gas chromatography-mass spectrometry-selected ion monitoring | en |
dc.type | Artigo | |
dcterms.license | http://www.elsevier.com/about/open-access/open-access-policies/article-posting-policy |