Comprehensive approach of methods for microstructural analysis and analytical tools in lignocellulosic biomass assessment – A review

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dc.contributor.authorRodrigues, Rita C.L.B.
dc.contributor.authorGreen Rodrigues, Bruna
dc.contributor.authorVieira Canettieri, Eliana [UNESP]
dc.contributor.authorAcosta Martinez, Ernesto
dc.contributor.authorPalladino, Fernanda
dc.contributor.authorWisniewski Jr, Alberto
dc.contributor.authorRodrigues Jr, Durval
dc.contributor.institutionUniversidade de São Paulo (USP)
dc.contributor.institutionUniversidade Estadual Paulista (UNESP)
dc.contributor.institutionState University of Feira de Santana (UEFS)
dc.contributor.institutionUniversidade Federal de Minas Gerais (UFMG)
dc.contributor.institutionUniversidade Federal de Sergipe (UFS)
dc.date.accessioned2022-04-29T08:39:23Z
dc.date.available2022-04-29T08:39:23Z
dc.date.issued2022-03-01
dc.description.abstractThe trend in the modern world is to replace fossil fuels with green energy sources in order to reduce their environmental impact. The biorefinery industry, within this premise, needs to establish quantitative and qualitative analytical methods to better understand lignocellulosic biomass composition and structure. This paper presents chemical techniques (chromatography, thermal analysis, HRMS, FTIR, NIR, and NMR) and physicochemical techniques (XRD, optical and electron microscopy techniques – Confocal fluorescence, Raman, SPM, AFM, SEM, and TEM) for the microstructural characterization of lignocellulosic biomass and its derivatives. Each of these tools provides different and complementary information regarding molecular and microstructural composition of lignocellulosic biomass. Understanding these properties is essential for the design and operation of associated biomass conversion processing facilities. PAT, monitored in real-time, ensures an economical and balanced mass-energy process. This review aimed to help researchers select the most suitable analytical technique with which to investigate biomass feedstocks with recalcitrant natures.en
dc.description.affiliationDepartament of Biotechnology Lorena Engineering School University of São Paulo (USP), 12600-970, SP
dc.description.affiliationChemistry and Energy Department Guaratinguetá Engineering Faculty São Paulo State University (UNESP), 12516-410, SP
dc.description.affiliationDepartment of Technology State University of Feira de Santana (UEFS), BA
dc.description.affiliationDepartment of Microbiology Institute of Biological Sciences Federal University of Minas Gerais (UFMG), MG
dc.description.affiliationDepartment of Chemistry Federal University of Sergipe (UFS), SE
dc.description.affiliationDepartment of Materials Engineering Lorena Engineering School University of São Paulo (USP), SP
dc.description.affiliationUnespChemistry and Energy Department Guaratinguetá Engineering Faculty São Paulo State University (UNESP), 12516-410, SP
dc.identifierhttp://dx.doi.org/10.1016/j.biortech.2021.126627
dc.identifier.citationBioresource Technology, v. 348.
dc.identifier.doi10.1016/j.biortech.2021.126627
dc.identifier.issn1873-2976
dc.identifier.issn0960-8524
dc.identifier.scopus2-s2.0-85124039077
dc.identifier.urihttp://hdl.handle.net/11449/230340
dc.language.isoeng
dc.relation.ispartofBioresource Technology
dc.sourceScopus
dc.subjectBiorefinery
dc.subjectLignin
dc.subjectProcess analytical technology
dc.subjectRecalcitrant feedstock
dc.subjectRenewable energy
dc.titleComprehensive approach of methods for microstructural analysis and analytical tools in lignocellulosic biomass assessment – A reviewen
dc.typeResenha
unesp.departmentFísica e Química - FEGpt

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Guaratinguetá - FEG - Faculdade de Engenharia e Ciências