Thermal and spectroscopic studies on solid Ketoprofen of lighter trivalent lanthanides

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dc.contributor.authorGalico, D. A. [UNESP]
dc.contributor.authorHolanda, B. B. [UNESP]
dc.contributor.authorPerpetuo, G. L. [UNESP]
dc.contributor.authorSchnitzler, E.
dc.contributor.authorTreu-Filho, O. [UNESP]
dc.contributor.authorBannach, Gilbert [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.contributor.institutionUniversidade Estadual de Ponta Grossa (UEPG)
dc.date.accessioned2014-05-20T13:26:54Z
dc.date.available2014-05-20T13:26:54Z
dc.date.issued2012-04-01
dc.description.abstractSolid-state Ln(L)(3) compounds, where Ln stands for trivalent La, Ce, Pr, Nd, Sm, Eu, and L is ketoprofen have been synthesized. Thermogravimetry (TG), differential thermal analysis (DTA), differential scanning calorimetry (DSC) as well as X-ray diffraction powder (DRX) patterns, Fourier transformed infrared spectroscopy (FTIR), and other methods of analysis were used to study solid Ketoprofen of lighter trivalent lanthanides. The results provided information of the composition, dehydration, coordination mode, structure, thermal behavior, and thermal decomposition. The theoretical and experimental spectroscopic study suggests that the carboxylate group of ketoprofen is coordinate to metals as bidentate bond.en
dc.description.affiliationUNESP, Fac Ciencias, Dept Quim, BR-17033260 Bauru, SP, Brazil
dc.description.affiliationUniversidade Estadual de Ponta Grossa (UEPG), Dept Quim, BR-84030900 Ponta Grossa, PR, Brazil
dc.description.affiliationUNESP, Inst Quim, BR-14800900 Araraquara, SP, Brazil
dc.description.affiliationUnespUNESP, Fac Ciencias, Dept Quim, BR-17033260 Bauru, SP, Brazil
dc.description.affiliationUnespUNESP, Inst Quim, BR-14800900 Araraquara, SP, Brazil
dc.description.sponsorshipFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
dc.description.sponsorshipFundação para o Desenvolvimento da UNESP (FUNDUNESP)
dc.description.sponsorshipPró-Reitoria de Pesquisa da UNESP (PROPe UNESP)
dc.description.sponsorshipConselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
dc.description.sponsorshipIdFAPESP: 10/10931-3
dc.format.extent371-379
dc.identifierhttp://dx.doi.org/10.1007/s10973-011-1866-1
dc.identifier.citationJournal of Thermal Analysis and Calorimetry. Dordrecht: Springer, v. 108, n. 1, p. 371-379, 2012.
dc.identifier.doi10.1007/s10973-011-1866-1
dc.identifier.issn1388-6150
dc.identifier.urihttp://hdl.handle.net/11449/8736
dc.identifier.wosWOS:000302704500050
dc.language.isoeng
dc.publisherSpringer
dc.relation.ispartofJournal of Thermal Analysis and Calorimetry
dc.relation.ispartofjcr2.209
dc.relation.ispartofsjr0,587
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectKetoprofenen
dc.subjectThermal behavioren
dc.subjectInfrared spectroscopyen
dc.subjectCarboxylate coordinationen
dc.titleThermal and spectroscopic studies on solid Ketoprofen of lighter trivalent lanthanidesen
dc.typeArtigo
dcterms.licensehttp://www.springer.com/open+access/authors+rights?SGWID=0-176704-12-683201-0
dcterms.rightsHolderSpringer
unesp.author.orcid0000-0002-8790-5069[6]
unesp.author.orcid0000-0001-9751-7951[2]
unesp.campusUniversidade Estadual Paulista (Unesp), Faculdade de Ciências, Baurupt
unesp.departmentQuímica - FCpt

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