Synthesis and sintering of ZrO2-CeO2 powder by use of polymeric precursor based on Pechini process
dc.contributor.author | Quinelato, A. L. | |
dc.contributor.author | Longo, Elson [UNESP] | |
dc.contributor.author | Leite, E. R. | |
dc.contributor.author | Bernardi, MIB | |
dc.contributor.author | Varela, José Arana [UNESP] | |
dc.contributor.institution | Comis Nacl Energia Atom | |
dc.contributor.institution | Universidade Federal de São Carlos (UFSCar) | |
dc.contributor.institution | Universidade Estadual Paulista (Unesp) | |
dc.date.accessioned | 2014-05-20T15:19:54Z | |
dc.date.available | 2014-05-20T15:19:54Z | |
dc.date.issued | 2001-01-01 | |
dc.description.abstract | Nanocrystalline ZrO2-12 mol % CeO2 powders were synthesized using a polymeric precursor method based on the Pechini process. X-ray diffraction (XRD) patterns showed that the method was effective to synthesize tetragonal zirconia single-phase. The mean crystallite size attained ranges from 6 to 15 nm. The BET surface areas were relatively high reaching 97 m(2)/g. Studies by nitrogen adsorption/desorption on powders, dilatometry of the compacts, and transmission electron microscopy (TEM) of the powders, were also developed to verify the particles agglomeration state. Both citric acid : ethylene glycol ratio and calcination temperature affected the powder morphology, which influenced the sinterability and microstructure of the sintered material, as showed by scanning electron microscopy (SEM). (C) 2001 Kluwer Academic Publishers. | en |
dc.description.affiliation | Comis Nacl Energia Atom, Lab Pocos Caldas, Rio Negro, MG, Brazil | |
dc.description.affiliation | Univ Fed Sao Carlos, Dept Quim, São Paulo, Brazil | |
dc.description.affiliation | Univ Estadual Paulista, Inst Quim, São Paulo, Brazil | |
dc.description.affiliationUnesp | Univ Estadual Paulista, Inst Quim, São Paulo, Brazil | |
dc.format.extent | 3825-3830 | |
dc.identifier | http://dx.doi.org/10.1023/A:1017950506356 | |
dc.identifier.citation | Journal of Materials Science. Dordrecht: Kluwer Academic Publ, v. 36, n. 15, p. 3825-3830, 2001. | |
dc.identifier.doi | 10.1023/A:1017950506356 | |
dc.identifier.issn | 0022-2461 | |
dc.identifier.uri | http://hdl.handle.net/11449/31282 | |
dc.identifier.wos | WOS:000169748400033 | |
dc.language.iso | eng | |
dc.publisher | Kluwer Academic Publ | |
dc.relation.ispartof | Journal of Materials Science | |
dc.relation.ispartofjcr | 2.993 | |
dc.relation.ispartofsjr | 0,807 | |
dc.rights.accessRights | Acesso restrito | |
dc.source | Web of Science | |
dc.title | Synthesis and sintering of ZrO2-CeO2 powder by use of polymeric precursor based on Pechini process | en |
dc.type | Artigo | |
dcterms.license | http://www.springer.com/open+access/authors+rights | |
dcterms.rightsHolder | Kluwer Academic Publ | |
unesp.campus | Universidade Estadual Paulista (Unesp), Instituto de Química, Araraquara | pt |
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