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Determination of the sodium monofluoroacetate in serum by gas chromatography

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dc.contributor.authorDemarchi, ACCO
dc.contributor.authorMenezes, Manoel Lima de [UNESP]
dc.contributor.authorMercadante, A.
dc.contributor.authorVassillief, I
dc.contributor.institutionUniversidade do Sagrado Coração (USC)
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2014-05-20T15:30:39Z
dc.date.available2014-05-20T15:30:39Z
dc.date.issued2001-09-01
dc.description.abstractSodium monofluoroacetate (NAFAc) has been widely used for vertebrate pest control, such as rabbits in Australia. However NAFAc is extremely toxic to all vertebrates and its use is restricted. Although this compound is stringently restricted, the occurrence of accidental and homicidal poisoning is no ever-present possibility.The method developed in this work shows the applicability of SPE with alumina cartridges for the extraction of NAFAc from serum samples. The method is efficient with recoveries of at least 96.8% from spiked serum. The samples were subsequently derivatized with dicyclohexylcabodiimide (DCC), using 2,4-dichloroaniline (DCA), to make the product volatile for GC analysis.en
dc.description.affiliationUniv Sagrado Coracao, Lab Anal & Pesquisas Clin, BR-17044160 São Paulo, Brazil
dc.description.affiliationUniv Estadual Paulista, Dept Quim, UNESP, BR-17033360 São Paulo, Brazil
dc.description.affiliationUniv Estadual Paulista, UNESP, Ctr Atendimento Toxicol, BR-18618000 São Paulo, Brazil
dc.description.affiliationUnespUniv Estadual Paulista, Dept Quim, UNESP, BR-17033360 São Paulo, Brazil
dc.description.affiliationUnespUniv Estadual Paulista, UNESP, Ctr Atendimento Toxicol, BR-18618000 São Paulo, Brazil
dc.format.extent402-404
dc.identifierhttp://dx.doi.org/10.1007/BF02492692
dc.identifier.citationChromatographia. Wiesbaden: Vieweg, v. 54, n. 5-6, p. 402-404, 2001.
dc.identifier.doi10.1007/BF02492692
dc.identifier.issn0009-5893
dc.identifier.lattes4659698040759224
dc.identifier.urihttp://hdl.handle.net/11449/39978
dc.identifier.wosWOS:000171316600020
dc.language.isoeng
dc.publisherVieweg
dc.relation.ispartofChromatographia
dc.relation.ispartofjcr1.401
dc.relation.ispartofsjr0,514
dc.rights.accessRightsAcesso restrito
dc.sourceWeb of Science
dc.subjectgas chromatographypt
dc.subjectsodium monofluoroacetatept
dc.subjectrodentspt
dc.subjectaluminapt
dc.titleDetermination of the sodium monofluoroacetate in serum by gas chromatographyen
dc.typeArtigo
dcterms.licensehttp://www.springer.com/open+access/authors+rights
dcterms.rightsHolderVieweg
dspace.entity.typePublication
unesp.author.lattes4659698040759224
unesp.campusUniversidade Estadual Paulista (UNESP), Faculdade de Ciências, Baurupt
unesp.departmentQuímica - FCpt

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