Thermal study of ZrO2 nanoparticles: Effect of heating and cooling cycles on solid-solid transition

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dc.contributor.authorGaglieri, Caroline [UNESP]
dc.contributor.authorAlarcon, Rafael T. [UNESP]
dc.contributor.authorde Godoi Machado, Rafael [UNESP]
dc.contributor.authorPadovini, David S.S. [UNESP]
dc.contributor.authorPontes, Fenelon M.L. [UNESP]
dc.contributor.authorCaires, Flávio J. [UNESP]
dc.contributor.institutionUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2018-12-11T16:46:57Z
dc.date.available2018-12-11T16:46:57Z
dc.date.issued2017-07-10
dc.description.abstractThis study investigates the influence of particle size on the solid-solid transition in zirconium (ZrO2) nanoparticles. The Simultaneous Thermogravimetry/Derivate Thermogravimetric-Differential Thermal Analysis (TG/DTG-DTA) was used to evince the phase transitions processes as well as the quantity of volatile compounds and the residual organic matter formed during the synthesis of nanoparticles. Field Emission Scanning Electron Microscopy (FE-SEM) and Transmission Electron Microscopy (TEM) were used to prove the increase and agglomeration;1;of particle size after each thermal cycle.en
dc.description.affiliationUniversidade Estadual Paulista (UNESP) Faculdade de Ciências
dc.description.affiliationUnespUniversidade Estadual Paulista (UNESP) Faculdade de Ciências
dc.description.sponsorshipCoordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
dc.description.sponsorshipFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
dc.format.extent59-61
dc.identifierhttp://dx.doi.org/10.1016/j.tca.2017.04.002
dc.identifier.citationThermochimica Acta, v. 653, p. 59-61.
dc.identifier.doi10.1016/j.tca.2017.04.002
dc.identifier.file2-s2.0-85017480030.pdf
dc.identifier.issn0040-6031
dc.identifier.scopus2-s2.0-85017480030
dc.identifier.urihttp://hdl.handle.net/11449/169634
dc.language.isoeng
dc.relation.ispartofThermochimica Acta
dc.relation.ispartofsjr0,605
dc.rights.accessRightsAcesso aberto
dc.sourceScopus
dc.subjectSolid-solid transition
dc.subjectThermal analysis
dc.subjectZrO2 nanoparticles
dc.titleThermal study of ZrO2 nanoparticles: Effect of heating and cooling cycles on solid-solid transitionen
dc.typeArtigo

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